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GCMS reference standard analysis, April 2002

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Quantitative results for reference standards analyzed by GCMS on April 3, 2002, to validate analytical accuracy.

NYC-WTC_000058911–000058918

Folder label: “GCMS X 3/8/02 A 3/30/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR3002\REFA2.D Vial: 28 Acq On : 30 Mar 2002 7:44 pm Operator: Sample : gc/ms scan 3/8 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 2 15:15 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.21 168 143802 7.71 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.30 248 106907 9.75' ug/1 # 89 32) Hexachlorobenzene 24.73 284 123969 9.74 ug/1 92 3 3) Phenanthrene 25.70 178 581978 9.76 ug/1 98 34) Anthracene 25.83 178 522408 8.83 ug/1 99 35) Di-n-butylphthalate 27.60 149 737960 9.83 ug/1 99 36) Fluoranthene 29.33 202 560274 8.95 ug/1 # 94 3 9) Pyrene 30.01 202 581574 13.57 ug/1 95 40) Butylbenzylphthalate 32.14 149 238380 10.79 ug/1 97 41) Benzo(a)anthracene 33.64 228 333602 9.36 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 288040 9.65 ug/1 95 43) Chrysene 33.77 228 365374 10.45 ug/1 99 45) Di-n-Octylphthalate 35.65 149 321498 8.64 ug/1 # 97 46) Benzo(b)fluoranthene 36.75 252 253469m 9.83 ug/1 47) Benzo(k)fluoranthene 36.82 252 290068m 11.54 ug/1 48) Benzo(a)pyrene 37.74 252 167829 7.14 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.06 276 182211 6.42 ug/1 97 50) Dibenz(a,h)anthracene 42.13 278 158787 7.23 ug/1 96 51) Benzo(g,h,i)perylene 43.30 276 158522 6.85 ug/1 97

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0308.M Tue Apr 02 15:16:33 2002 Page 2

NYC-WTC_000058917

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NYC-WTC_000058917Source: NYC Law Department, mirrored locally

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