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GCMS reference standard results for sample AE04803, April 2002

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Laboratory report listing concentrations of target analytes in a reference standard analyzed on April 2, 2002.

NYC-WTC_000058498–000058505

Folder label: “GCMS X 3/5/02 A 3/29/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2802\REFA2.D . Vial: 17 Acq On : 29 Mar 2002 12:24 am Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 14:57 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.21 168 124301 7.57 ug/1 # 83 31) 4-Bromophenyl-phenylether 24.29 248 104034 10.78 ug/1 92 32) Hexachlorobenzene 24.73 284 124746 11.13 ug/1 # 89 3 3) Phenanthrene 25.70 178 570320 10.87 ug/1 99 34) Anthracene 25.84 178 496081 9.53 ug/1 98 35) Di-n-butylphthalate 27.60 149 735155 11.13 ug/1 99 36) Fluoranthene 29.33 202 552490 10.03 ug/1 # 94 3 9) Pyrene 30.00 202 565594 14.87 ug/1 95 40) Butylbenzylphthalate 32: 13 149 243567 12.42 ug/1 96 41) Benzo(a)anthracene 33.64 228 324298 10.25 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 300820 11.36 ug/1 95 43) Chrysene 33.77 228 355830 11.47 ug/1 99 45) Di-n-Octylphthalate 35.65 149 329199 10.31 ug/1 # 98 46) Benzo(b)fluoranthene 36.75 252 244626 11.06 ug/1 98 47) Benzo(k)fluoranthene 36.82 252 263295 12.21 ug/1 98 48) Benzo(a)pyrene 37.74 252 165055 8.19 ug/1 98 49) Indeno(1,2,3-cd)pyrene 42.06 276 165625 6.80 ug/1 97 50) Dibenz(a,h)anthracene 42.13 278 148151 7.86 ug/1 97 51) Benzo(g,h,i)perylene 43.30 276 • 146630■ 7.38 ug/1 98

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0308.M Mon Apr 01 15:00:10 2002 Page 2

NYC-WTC_000b58501

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NYC-WTC_000058501Source: NYC Law Department, mirrored locally

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