GCMS reference standard results for sample AE04803, April 2002

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2802\REFA2.D Vial: 17 Acq On : 29 Mar 2002 12:24 am . Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 14:57 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 402934 20.00 ug/1 -0.10 10) Naphthalene-d8 15'.89 136 1480125 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.19 164 849422 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.63 188 1215268 20.00 ug/1 -0.13 38) Chrysene-dl2 33.69 240 • 662313 20.00 ug/1 -0.15 44) Perylene-dl2 37.94 264 362239 20.00 ug/1 -0.19

System Monitoring Compounds 37) 2,4-DDD 30.71 235 81676 <€i^?0"ug/mL 0.21 Spiked Amount 5.000 Recovery

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 78484 5.74 ug/1 # 68 3) bis(2-Chloroethyl)ether 11.64 93 192986 8.77 ug/1 91 4) 1,3-Dichlorobenzene 12.15 146 131736 5.79 ug/1 99 5) 1,4-Dichlorobenzene 12.30 146 141132 6.19 ug/1 99 6) 1,2-Dichlorobenzene 12.81' 146 143441 6.75 ug/1 97 7) 2,2'-oxybis(1-Chloropropan 13.13 45 271343 8.76 ug/1 98 8) N-Nitroso-di-n-propylamine 13.52 70 127975 8.94 ug/1 # 85 9) Hexachloroethane 13.66 117 35599 4.18 ug/1 96 11) Nitrobenzene 13 .'93 77 175568 8.68 ug/1 93 12) Isophorone 14.57 82 399887 10.42 ug/1 100 13) bis(2-Chloroethoxy)methane 15.26 93 244181 9.72 ug/1 98 14) 1,2,4-Trichlorobenzene 15.78 180 130512 7.51 ug/1 93 15) Naphthalene 15.94 128 512273 . 9.36 ug/1 99 16) Hexachlorobutadiene 16.49 225 33568 3.88 ug/1 99 18) Hexachlorocyclopentadiene 18.69 237 12513 2.18 ug/1 # 97 19) 2-Chloronaphthalene 19.45 162 320877 8.80 ug/1 96 20) Dimethylphthalate 20.54 163 459332 10.75 ug/1 100 21) 2,6-Dinitrotoluene 20.75 165 93939 9.05 ug/1 # 81 22) Acenaphthylene 20.72 152 523761 10.05 ug/1 100 23) Acenaphthene 21.28 153 361654 9.92 ug/1 98 24) 2,4-Dinitrotoluene 21.92 165 119713 8.62 ug/1 # 78 25) Diethylphthalate 22.67 149 448101 10.80 ug/1 95 26) 4-Chlorophenyl-phenylether 22.83 204 189129 10.64 ug/1 91 27) Fluorene 22.81 166 404378 10.49 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 23.29 77 379677 8.54 ug/L # 81

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0308.M Mon Apr 01 15:00:01 2002 Page 1

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