GCMS reference analysis results, sample AE05231, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR3OO2\REFB1.D Vial: 40 Acq On : 31 Mar 2002 7:39 am Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 3 13:36 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.24 152 414039 20.00 ug/1 -0.11 10) Naphthalene-d8 15.88 136 1514896 20.00 ug/1 -0.12 17) Acenaphthene-dlO 21.19 164 871571 20.00 ug/1 -0.13 29) Phenanthrene-dlO 25.63 188 1236867 20.00 ug/1 -0.14 38) Chrysene-dl2 33.69 240 654064 20.00 ug/1 -0.15 44) Perylene-dl2 37.93 264 362026 20.00 ug/1 -0.19

System Monitoring Compounds 37) 2,4-DDD 30.71 235 76238 6.14 ug/mL 0.21 Spiked Amount 5.000 Recovery 122.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.88 74 74212 5.28 ug/1 # 66 3) bis(2-Chloroethyl)ether 11.64 93 180191 7.97 ug/1 91 4) 1,3-Dichlorobenzene 12.15 146 154968 6.63 ug/1 98 5) 1,4-Dichlorobenzene 12.29 146 161806 6.91 ug/1 98 6) 1,2-Dichlorobenzene 12.80 146 157465 7.21 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.13 45 247058 7.76 ug/1 98 8) N-Nitroso-di-n-propylamine 13.51 70 117642 7.99 ug/1 # 84 9) Hexachloroethane 13.66 117 48516 5.54 ug/1 99 11) Nitrobenzene 13.92 77 161135 7.78 ug/1 92 12) Isophorone 14.58 82 353407 9.00 ug/1 98 13) bis(2-Chloroethoxy)methane 15.26 93 221254 8.61 ug/1 98 14) 1,2,4-Trichlorobenzene 15.77 180 141628 7.96 ug/1 97 15) Naphthalene 15.94 128 490889 8.77 ug/1 99 16) Hexachlorobutadiene 16.49 225 54048 6.10 ug/1 98 18) Hexachlorocyclopentadiene 18.68 237 19188 3.25 ug/1 98 19) 2-Chloronaphthalene 19.44 162 311691 8.33 ug/1 95 20) Dimethylphthalate 20.53 163 425835 9.71 ug/1 98 21) 2,6-Dinitrotoluene 20.75 165 82610 7.76 ug/1 # 82 22) Acenaphthylene 20.72 152 473389 8.85 ug/1 100 2 3) Acenaphthene 21.28 153 335890 8.98 ug/1 98 24) 2,4-Dinitrotoluene 21.92 165 105156 7.38 ug/1 # 74 25) Diethylphthalate 22.66 149 410957 9.65 ug/1 95 26) 4-Chlorophenyl-phenylether 22.82 204 181892 9.98 ug/1 91 27) Fluorene 22.80 166 375409 9.49 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.29 77 340256 7.46 ug/L # 83

(#) = qualifier out of range (m) = manual integration REFBl.D GCMS0308.M Wed Apr 03 13:37:14 2002 Page 1

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