GCMS calibration results, sample AE05035, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR3002\REFl.D Vial: 17 Acq On : 30 Mar 2002 6:51 am Operator: Sample : gc/ms scan 3/7 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 30 7:39 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth ; GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 513280 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 1856731 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.19 164 1061461 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.63 188 1527208 20.00 ug/1 -0.13 38) Chrysene-dl2 33.69 •24 0 802109 20.00 ug/1 -0.15 44) Perylene-dl2 37.94 264 425496 20.00 ug/1 -0.19

System Monitoring Compounds 37) 2,4-DDD 30.71 23 5 84212 5.50 ug/mL 0.21 Spiked Amount 5.000 Recovery = 110.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 83863 4.82 ug/1 # 72 3) bis(2-Chloroethyl)ether 11.64 93 210636 7.51 ug/1 90 4) 1,3-Dichlorobenzene 12.15 146 183764 6.'34 ug/1 97 5) 1,4-Dichlorobenzene 12.30 146 190470 6.56 ug/1 99 6) 1,2-Dichlorobenzene 12.81 146 188887 6.97 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.13 45 290311 7.36 ug/1 99 8) N-Nitroso-di-n-propylamine 13.52 70 139187 7.63 ug/1 # 85 9) Hexachloroethane 13.66 117 57044 5.26 ug/1 88 11) Nitrobenzene 13.93 77 191695 7.55 ug/1 92 12) Isophorone 14.57 82 415260 8.63 ug/1 99 13) bis(2-Chloroethoxy)methane 15.26 93 258284 8.20 ug/1 97 14) 1,2,4-Trichlorobenzene 15.77 180 170295 7.81 ug/1 97 15) Naphthalene 15.94 128 586488 8.55 ug/1 99 16) Hexachlorobutadiene 16.48 225 65483 6.03 ug/1 98 18) Hexachlorocyclopentadiene 18.69 237 18805 2.62 ug/1 96 19) 2-Chloronaphthalene 19.45 162 370215 8.12 ug/1 95 20) Dimethylphthalate 20.53 163 481627 9.02 ug/1 99 21) 2,6-Dinitrotoluene 20.75 165 98590 7.60 ug/1 # 81 22) Acenaphthylene 20.72 152 558057 8.57 ug/1 99 23) Acenaphthene 21.28 153 389580 8.56 ug/1 98 24) 2,4-Dinitrotoluene 21.92 165 122332 7.05 ug/1 # 78 25) Diethylphthalate 22.67 149 458483 8.84 ug/1 # 94 26) 4-Chlorophenyl-phenylether 22.83 204 210362 9.47 ug/1 89 27) Fluorene 22.81 166 433563 9.00 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.28 77 388543 6.99 ug/L # 85

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0308.M Tue Apr 02 13:52:50 2002 Page 1

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