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GCMS calibration results, sample AE05035, April 2002

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Laboratory report showing GCMS calibration analysis for volatile organic compounds on April 2, 2002.

NYC-WTC_000058826–000058837

Folder label: “GCMS X 3/7/02 A 3/30/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR3002\REFl.D Vial: 17 Acq On : 30 Mar 2002 6:51 am Operator: Sample : gc/ms. scan 3/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 30 7:39 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenyiamine 23.21 168 152721 7.40 ug/1 # 82 31) 4-Bromophenyl-phenylether 24.29 248 115171 9.50 ug/1 # 88 32) Hexachlorobenzene 24.73 284 139881 9.94 ug/1 # 88 33) Phenanthrene 25.70 178 596167 9.04 ug/1 99 34) Anthracene 25.83 178 507834 7.76 ug/1 98 35) Di-n-butylphthalate 27.60 149 743626 8.96 ug/1 99 36) Fluoranthene 29.33 202 569748 8.23 ug/1 95 39) Pyrene 30.00 202 512067 11.12 ug/1 95 40) Butylbenzylphthalate 32.13 149 234172 9.86 ug/1 # 95 41) Benzo(a)anthracene 33.64 228 313826 8.19 ug/1 ■ 99 42) Bis(2-ethylhexyl)phthalate 33.91 14 9 276355 8.62 ug/1 94 43) Chrysene 33.77 228 355218 9.46 ug/1 99 45) Di-n-Octylphthalate 35.65 149 293425 7.83 ug/1 # 97 46) Benzo(b)fluoranthene 36.74 252 236301 9.09 ug/1 98 47) Benzo(k)fluoranthene 36.82 252 278643 11.00 ug/1 98 48) Benzo(a)pyrene 37.73 252 150564 6.36 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.05 276 145533 5.09 ug/1 95 50) Dibenz(a,h)anthracene 42.12 278 125155 5.65 ug/1 96 51) Benzo(g,h,i)perylene 43.29 276 131349 5.63 ug/1 96

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0308.M Tue Apr 02 13:52:54 2002 Page 2

NYC-WTC_000058833

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NYC-WTC_000058833Source: NYC Law Department, mirrored locally

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