Calibration results for specific volatile organic compounds used to verify GCMS instrument performance in April 2002.
NYC-WTC_000059118–000059125Folder label: “GCMS X 3/9/02 A 3/30/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\MAR3 002\REFBl.D Vial: 40 Acq On 31 Mar 2002 . 7:39 am Operator: Sample gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 3 13:36 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 23.22 168 128861 7.71 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.29 248 100500 10.24 ug/1 # 90 32) Hexachlorobenzene 24.73 284 124083 10.88 ug/1 # 86 33) Phenanthrene 25.69 178 527276 9.87 ug/1 98 34) Anthracene 25.83 178 476926 9.00 ug/1 98 35) Di-n-butylphthalate 27.60 149 666822 9.92 ug/1 # 98 36) Fluoranthene 29.32 202 494913 8.83 ug/1 # 93 3 9) Pyrene 30.00 202 509503 13.57 ug/1 # 94 40) Butylbenzylphthalate 32.13 14 9 205124 10.59 ug/1 # 98 41) Benzo(a)anthracene 33.63 228 284178 9.10 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 266169 10.18 ug/1 93 43) Chrysene 33.76 228 315929 10.31 ug/1 98 45) Di-n-Octylphthalate 35.65 149 275363 8.63 ug/1 # 97 46) Benzo(b)fluoranthene 36.75 252 206795 9.35 ug/1 98 47) Benzo(k)fluoranthene 36.81 252 233370m 10.83 ug/1 48) Benzo(a)pyrene 37.74 252 149600 7.42 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.04 276 145584 5.98 ug/1 9'6 50) Dibenz(a,h)anthracene 42.13 278 126672 6.73 ug/1 # 95 51) Benzo(g,h,i)perylene 43.28 276 131678 6.64 ug/1 96
{#) = qualifier out of range (m) = manual integration REFBl.D GCMS0308.M Wed Apr 03 13:37:18 2002 Page 2
NYC-WTC_000059124
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NYC-WTC_000058911
Quantitative results for reference standards analyzed by GCMS on April 3, 2002, to validate analytical accuracy.
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Laboratory report showing GCMS calibration analysis for volatile organic compounds on April 2, 2002.
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Laboratory report listing concentrations of target analytes in a reference standard analyzed on March 29, 2002.
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Reference standard analysis for gas chromatography-mass spectrometry dated March 29, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059491
Calibration data sheet listing retention times and response factors for multiple organic compounds analyzed on April 5, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058175
Analysis of reference standards for nitrosamines and VOCs with measured concentrations near target levels on March 29, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059222
Reference standard analysis report for volatile organic compounds using GCMS on April 4, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058258
Reference standard analysis report for sample AE04733 conducted April 1, 2002, listing concentrations of quality control compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058498
Laboratory report listing concentrations of target analytes in a reference standard analyzed on April 2, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011849
Reference analysis record for GCMS testing of sample AE04388 conducted on March 28, 2002, by analyst MG.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011711
Calibration record for GCMS analysis of sample AE04038 conducted on March 27, 2002, showing compound responses.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010289
Reference data report displaying measured concentrations and detection limits for target analytes analyzed on March 21, 2002.
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Laboratory report showing non-detect levels for various organic compounds in a GCMS blank sample from April 2002.
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NYC-WTC_000059114
Calibration results for specific volatile organic compounds used to verify GCMS instrument performance in April 2002.
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NYC-WTC_000059126
Laboratory report documenting GCMS analysis of sample AE05231 for unknown compounds on April 9, 2002.
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