GCMS reference standard results for sample AE04803, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR28O2\REFA1.D Vial: 16 Acq On : 28 Mar 2002 11:25 pm Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 ' Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 14:56 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 407211 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 1491348 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.19 164 858384 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.64 188 1236629 20.00 ug/1 -0.13 38) Chrysene-dl2 33.70 240 678119 20.00 ug/1 -0.15 44) Perylene-dl2 37.94 264 378367 20.00 ug/1 -0.18

System Monitoring Compounds 7/ 37) 2,4-DDD 30.71 235 81480 ug/mL 0.22 Spiked Amount 5.000 Recovery Y’/Y

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 90807 6.57 ug/1 # 67 3) bis(2-Chloroethyl)ether 11.65 93 225056 10.12 ug/1 90 4) 1,3-Dichlorobenzene 12.15 146 187514 8.16 ug/1 99 5) 1,4-Dichlorobenzene 12.29 146 196771 8.54 ug/1 99 6) 1,2-Dichlorobenzene 12.81 146 194182 9.04 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.12 45 309056 9.87 ug/1 98 8) N-Nitroso-di-n-propylamine 13.51 70 145276 10.04 ug/1 . 88 9) Hexachloroethane 13.66 117 56157 6.52 ug/1 98 11) Nitrobenzene 13.93 77 201444 9.88 ug/1 89 12) Isophorone 14.57 82 448037 11.59 ug/1 98 13) bis(2-Chloroethoxy)methane 15.25 93 271739 10.74 ug/1 96 14) 1,2,4-Trichlordbenzene 15.77 180 173024 9.88 ug/1 99 15) Naphthalene 15.94 128 605853 10.99 ug/1 99 16) Hexachlorobutadiene 16.48 225 60628 6.95 ug/1 100 18) Hexachlorocyclopentadiene 18.68 237 21637 3.72 ug/1 93 19) 2-Chloronaphthalene 19.45 162 374031 10.15 ug/1 95 20) Dimethylphthalate 20.53 163 489313 11.33 ug/1 99 21) 2,6-Dinitrotoluene 20.75 165 98909 9.43 ug/1 # 81 22) Acenaphthylene • 20.72 152 570186 10.82 ug/1 98 23) Acenaphthene 21.29 153 396027 10.75 ug/1 98 24) 2,4-Dinitrotoluene 21.92 165 124390 8.87 ug/1 # 76 25) Diethylphthalate 22.67 149 476693 11.37 ug/1 95 26) 4-Chlorophenyl-phenylether 22.83 204 215164 11.98 ug/1 91 27) Fluorene 22.80 166 440799 11.32 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.29 77 407946 9.08 ug/L # 86

(#) = qualifier out of range (m) = manual integration REFAl.D GCMS0308.M Mon Apr 01 14:56:50 2002 Page 1

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