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GCMS reference standard results for sample AE04803, April 2002

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Laboratory report listing concentrations of target analytes in a reference standard analyzed on April 2, 2002.

NYC-WTC_000058498–000058505

Folder label: “GCMS X 3/5/02 A 3/29/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR28O2\REFA1.D Vial: 16 Acq On : 28 Mar 2002 11:25 pm Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 14:56 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS03 08.M (RTE Integrator)- Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.21 168 143021 8.56 ug/1 # 80 31) 4-Bromophenyl-phenylether 24.30 248 117081 11.93 ug/1 # 89 32) Hexachlorobenzene 24.73 284 143344 12.57 ug/1 # 89 3 3) Phenanthrene 25.70 178 616395 11.54 ug/1 99 34) Anthracene 25.83 178 546372 10.31 ug/1 98 35) Di-n-butylphthalate 27.60 149 770949 11.47' ug/1 99 36) Fluoranthene 29.33 202 590627 10.54 ug/1 # 95 3 9) Pyrene 30.00 202 605010 15.54 ug/1 # 92 40) Butylbenzylphthalate 32.13 149 253575 12.63 ug/1 98 41) Benzo(a)anthracene 33.64 228 342097 10.56 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.91 149 313073 11.55 ug/1 95 43) Chrysene 33.77 228 378298 11.91 ug/1 99 45) Di-n-Octylphthalate 35.65 149 350618 10.52 ug/1 # 96 46) Benzo(b)fluoranthene 36.75 252 266234m 11.52 ug/1 47) Benzo(k)fluoranthene 36.82 252 276105 12.26 ug/1 98 48) Benzo(a)pyrene 37.74 252 179838 8.54 ug/1 # 97 49) Indeno(l,2,3-cd)pyrene 42.05 276 181558 7.14 ug/1 98 50) Dibenz(a,h)anthracene 42.13 278 154803 7.86 ug/1 96 51) Benzo(g,h,i)perylene 43.29 276 160441 7.74 ug/1 97

(#) = qualifier out of range (m) = manual integration REFAl.D GCMS0308.M Mon Apr 01 14:56:53 2002 Page 2

NYC-WTC_000058504

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NYC-WTC_000058504Source: NYC Law Department, mirrored locally

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