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GCMS analysis results for sample AE01156, March 29 2002

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Gas chromatography-mass spectrometry analysis of sample AE01156 conducted March 29, 2002, showing surrogate standard 2,4-DDD recovery.

NYC-WTC_000059687–000059692

Folder label: “GCMS X 3/13/02 A 3/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR21O2\REFA1.D Vial: 17 Acq On : 22 Mar 2002 3:04 am Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 25 8:51 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30)■N-Nitrosodiphenylamine 23.24 168 138873 9.16 ug/1 # 80 31) 4-Bromophenyl-phenylether 24.31 248 97920 10.99 ug/1 93 32) Hexachlorobenzene 24.75 284 115833 11.20 ug/1 # 89 3 3) Phenanthrene 25.73 178 536900 11.08 ug/1 99 34) Anthracene 25.85 178 501054 10.43 ug/1 99 35) Di-n-butylphthalate 27.63 149 690764 11.33 ug/1 99 36) Fluoranthene 29.35 202 542332 10.67 ug/1 95 39) Pyrene 30.02 202 561243 13.62 ug/1 # 91 40) Butylbenzylphthalate 32.15 149 251510 11.84 ug/1 97 41) Benzo(a)anthracene 33.67 228 369171 10.77 ug/1 99 42) Bis (2-ethylhexyl) phthalate' 33.93 149 333414 11.62 ug/1 95 43) Chrysene 33.80 228 390911 11.63 ug/1 98 45) Di-n-Octylphthalate 35.68 149 398311 10.39 ug/1 # 97 46) Benzo(b)fluoranthene 36.78 252 310764 11.70 ug/1 98 47) Benzo (]<) fluoranthene 36.84 252 334880 12.93 ug/1 98 48) Benzo(a)pyrene 37.77 252 219098 9.05 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.11 276 234318 8.02 ug/1 95 50) Dibenz(a,h)anthracene 42.19 278 200509 8.86 ug/1 98 51) Benzo (g, h, D perylene 43.35 276 206983 8.68 ug/1 96

(#) .= qualifier out of range (m) = manual integration REFAl.D GCMS0308.M Mon Mar 25 09:00:48 2002 Page 2

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NYC-WTC_000059688Source: NYC Law Department, mirrored locally

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