GCMS analysis results for sample AE01156, March 29 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR21O2\REFA1.D Vial: 17 Acq On : 22 Mar 2002 3:04 am Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 25 8:51 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.27 152 353974 20.00 ug/1 -0.09 10) Naphthalene-d8 15.90 136 1390700 20.00 ug/1 -0.09 17) Acenaphthene-dlO 21.21 164 759669 20.00 ug/1 -0.10 29) Phenanthrene-dlO 25.65 188 1121912 20.00 ug/1 -0.11 38) Chrysene-dl2 33.72 240 717540 20.00 ug/1 -0.12 44) Perylene-dl2 37.97 264 434961 20.00 ug/1 -0.15

System Monitoring Compounds 37) 2,4-DDD 30.74 235 79231 9.72 ug/mL 0.24 Spiked Amount 5.000 Recovery = 194.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.90 74 77250 6.43 ug/1 # 69 3) bis(2-Chloroethyl)ether 11.65 93 187068 9.67 ug/1 92 4) 1,3-Dichlorobenzene 12.17 146 166111 8.31 ug/1 99 5) 1,4-Dichlorobenzene 12.30 146 172833 8.63 ug/1 100 6) 1,2-Dichlorobenzene 12.83 146 168674 9.03 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 13.14 45 261593 9.61 ug/1 99 8) N-Nitroso-di-n-propylamine 13.53 70 126493 10.05 ug/1 # 88 9) Hexachloroethane 13.67 117 54542 7.29 ug/1 96 11) Nitrobenzene 13.95 77 168814 8.88 ug/1 90 12) Isophorone 14.59 82 361943 10.04 ug/1 98 13) bis(2-Chloroethoxy)methane 15.28 93 228031 9.66 ug/1 98 14) 1,2,4-Trichlorobenzene 15.79 180 149599 9.16 ug/1 98 15) Naphthalene 15.96 128 515542 10.03 ug/1 99 16) Hexachlorobutadiene 16.51 225 59946 7.37 ug/1 99 18) Hexachlorocyclopentadiene 18.70 237 20106 3.91 ug/1 96 19) 2-Chloronaphthalene 19.47 162 310918 9.53 ug/1 96 20) Dimethylphthalate 20.56 163 421135 11.02 ug/1 . 99 21) 2,6-Dinitrotoluene 20.77 165 85634 9.23 ug/1 # 86 22) Acenaphthylene 20.74 152 481080 10.32 ug/1 98 23) Acenaphthene 21.30 153 334837 10.27 ug/1 99 24) 2,4-Dinitrotoluene 21.94 165 106398 8.57 ug/1 # 74 25) Diethylphthalate 22.69 149 414799 11.18 ug/1 96 26) 4-Chlorophenyl-phenylether 22.84 204 184035 11.58 ug/1 94 27) Fluorene 22.83 166 379346 11.01 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.31 77 354487 8.91 ug/L # 84

(#) = qualifier out of range (m) = manual integration REFAl.D GCMS0308.M Mon Mar 25 09:00:44 2002 Page 1

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