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GCMS reference results, Sample AE04417, Mar 2002

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Laboratory report for GC/MS reference analysis of sample AE04417 conducted on March 22, 2002.

NYC-WTC_000012309–000012316

Folder label: “GCMS X 3-1-02 A 3-21-02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2102\REF2.D Vial: 5 Acq On : 21 Mar 2002 3:12 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 22 8:54 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.23 168 147416 5.34 ug/1 # 85 31) 4-Bromophenyl-phenylether 24.31 248 96531 5.95 ug/1 92 3 2) Hexachlorobenzene 24.75 284 109378 5.80 ug/1 94 3 3) Phenanthrene 25.73 178 534069 6.05 ug/1 98 34) Anthracene 25.86 178 480015 5.48 ug/1 99 35) Di-n-butylphthalate 27.62 149 665563 5.99 ug/1 99 36) Fluoranthene 29.35 202 529014 5.71 ug/1 # 92 3 9) Pyrene 30.02 202 551004 6.98 ug/1 # 93 40) Butylbenzylphthalate 32.15 149 247950 6.09 ug/1 99 41) Benzo(a)anthracene 33.67 228 379271 5.78 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.94 149 335733 6.11 ug/1 95 43) Chrysene 33.80 228 406984 6.32 ug/1 100 45) Di-n-Octylphthalate 35.67 149 435605 5.57 ug/1 99 46) Benzo(b)fluoranthene 36.85 252 349711 6.45 ug/1 98 47) Benzo(k)fluoranthene 36.85 252 323506 6.12 ug/1 98 4 8) Benzo(a)pyrene 37.77 252 212743 4.31 ug/1 # 96 4 9) Indeno(1,2,3-cd)pyrene 42.11 276 272537 4.57 ug/1 97 50) Dibenz(a,h)anthracene 42.19 278 240900 5.22 ug/1 96 51) Benzo(g,h,i)perylene 43.35 276 235558 4.84 ug/1 93

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0308.M Fri Mar 22 09:01:49 2002 Page 2

NYC-WTC_000012315

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NYC-WTC_000012315Source: NYC Law Department, mirrored locally

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