GCMS reference results, Sample AE04417, Mar 2002

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2102\REF2.D Vial: 5 Acq On : 21 Mar 2002 3:12 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 22 8:54 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.26 152 646636 20.00 ug/1 -0.09 10) Naphthalene-d8 15.91 136 2522005 20.00 ug/1 -0.09 17) Acenaphthene-diO 21.22 164 1352406 20.00 ug/1 -0.09 29) Phenanthrene-diO 25.66 188 2044922 20.00 ug/1 -0.10 38) Chrysene-dl2 33.72 240 1374681 20.00 ug/1 -0.12 44) Perylene-dl2 37.98 264 887365 20.00 ug/1 -0.14

System Monitoring Compounds 37) 2,4-DDD 30.73 235 75729 5.10 ug/mL 0.23 Spiked Amount 5.000 Recovery = 102.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 81320 3.71 ug/1 # 71 3) bis(2-Chloroethyl)ether 11.65 93 185836 5.26 ug/1 92 4) 1,3-Dichlorobenzene 12.16 146 142124 3.89 ug/1 99 5) 1,4-Dichlorobenzene 12.31 146 150320 4.11 ug/1 99 6) 1,2-Dichlorobenzene 12.82 146 152061 4.46 ug/1 98 7) 2,2'-oxybi s(1-Chioropropan 13.14 45 260835 5.25 ug/1 98 8) N-Nitroso-di-n-propylamine 13.53 70 130646 5.68 ug/1 # 86 9) Hexachloroethane 13.67 117 41472 3.03 ug/1 97 11) Nitrobenzene 13.94 77 171354 4.97 ug/1 92 12) Isophorone 14.59 82 383539 5.87 ug/1 98 13) bis(2-Chloroethoxy)methane 15.27 93 227509 5.32 ug/1 98 14) 1,2,4-Trichlorobenzene 15.79 180 133943 4.52 ug/1 99 15) Naphthalene 15.96 128 497887 5.34 ug/1 99 16) Hexachlorobutadiene 16.50 225 35506 2.41 ug/1 98 18) Hexachlorocyclopentadiene 18.71 237 8630 0.94 ug/1 97 19) 2-Chioronaphthalene 19.47 162 303087 5.22 ug/1 97 20) Dimethylphthalate 20.55 163 409906 6.02 ug/1 99 21) 2,6-Dinitrotoluene 20.77 165 85458 5.17 ug/1 # 83 2 2) Acenaphthylene 20.74 152 477230 5.75 ug/1 99 2 3) Acenaphthene 21.30 153 328337 5.66 ug/1 98 24) 2,4-Dinitrotoluene 21.94 165 109212 4.94 ug/1 # 80 25) Diethylphthalate 22.69 149 398966 6.04 ug/1 97 26) 4-Chlorophenyl-phenylether 22.85 204 177806 6.28 ug/1 92 27) Fluorene 22.83 166 369804 6.03 ug/1 99 2 8) Azobenzen/ 1,2-Diphenylhyd 23.31 77 352652 4.98 ug/L # 85

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0308.M Fri Mar 22 09:01:46 2002 Page 1

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