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GCMS reference results for sample AE02567, March 2002

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Laboratory report listing quantitative results for volatile organic compounds in sample AE02567 analyzed on March 21, 2002.

NYC-WTC_000038756–000038763

Folder label: “GCMS X 3/4/02 A 3/20/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR19O2\REFA1.D Vial: 17 Acq On : 20 Mar 2002 8:44 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 21 13:45 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.24 168 181549 7.06 ug/1 # 80 31) 4-Bromophenyl-phenylether 24.31 248 107814 7.13 ug/1 94 32) Hexachlorobenzene 24.75 284 111012 6.33 ug/1 92 33) Phenanthrene 25.73 178 645117 7.85 ug/1 98 34) Anthracene 25.85 178 605667 7.43 ug/1 98 35) Di-n-butylphthalate 27.63 149 865293 8.36 ug/1 99 36) Fluoranthene 29.35 202 685182 7.94 ug/1 95 3 9) Pyrene 30.03 202 720107 9.54 ug/1 94 40) Butylbenzylphthalate 32.15 149 332202 8.54 ug/1 96 41) Benzo(a)anthracene 33.67 228 522238 8.32 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.93 149 440739 8.39 ug/1 96 43) Chrysene 33.80 228 550724 8.95 ug/1 99 45) Di-n-Octylphthalate 35.67 149 583750 7.98 ug/1 # 98 46) Benzo(b)fluoranthene 36.78 252 433956 8.57 ug/1 98 47) Benzo(k)fluoranthene 36.84 252 446990m 9.05 ug/1 48) Benzo(a)pyrene 37.77 252 336860 7.30 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.11 276 369516 6.63 ug/1 96 50) Dibenz(a,h)anthracene 42.19 278 312507 7.24 ug/1 96 51) Benzo(g,h,i)perylene 43.35 276 320072 7.04 ug/1 94

(#) = qualifier out of range (m) = manual integration REFA1.D GCMS0308.M Thu Mar 21 13:46:32 2002 Page 2

NYC-WTC_000038762

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NYC-WTC_000038762Source: NYC Law Department, mirrored locally

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