GCMS analysis results for sample AE01156, March 29 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2102\REFA2.D Vial: 18 Acq On : 22 Mar 2002 4:03 am Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 25 9:01 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 383979 20.00 ug/1 -0.09 10) Naphthalene-d8 15.90 136 1463168 20.00 ug/1 -0.10 17) Acenaphthene-dlO 21.21 164 800622 20.00 ug/1 -0.10 29) Phenanthrene-dlO 25.66 188 1207349 20.00 ug/1 -0.11 38) Chrysene-dl2 33.72 240 765806 .20.00 ug/1 -0.13 44) Perylene-dl2 37.97 264 459923 20.00 ug/1 -0.15

System Monitoring Compounds 37) 2,4-DDD 30.73 235 61427 7.00 ug/mL 0.24 Spiked Amount 5.000 Recovery = 140.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.90 74 60556 4.65 ug/1 # 71 3) bis(2-Chloroethyl)ether 11.66 93 150373 7.17 ug/1 93 4) 1,3-Dichlorobenzene 12.16 146 129510 5.97 ug/1 99 5) 1,4-Dichlorobenzene 12.31 146 134278 6.18 ug/1 99 6) 1,2-Dichlorobenzene 12.82 146 133230 6.57 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.15 45 212629 7.20 ug/1 98 8) N-Nitroso-di-n-propylamine 13.53 70 100975 7.40 ug/1 # 86 9) Hexachloroethane 13.68 117 40951 5.04 ug/1 92 11) Nitrobenzene 13.94 77 136568 6.83 ug/1 96 12) Isophorone 14.60 82 286857 7.56 ug/1 100 13) bis(2-Chloroethoxy)methane 15.28 93 188531 7.59 ug/1 98 14) 1,2,4-Trichlorobenzene 15.79 180 116796 6.80 ug/1 97 15) Naphthalene 15.96 128 409224 7.57 ug/1 100 16) Hexachlorobutadiene 16.51 225 46127 5.39 ug/1 96 ■18) Hexachlorocyclopentadiene 18.70 237 15192 2.80 ug/1 97 19) 2-Chloronaphthalene 19.47 162 253520 7.38 ug/1 96 20) Dimethylphthalate 20.55 163 344453 8.55 ug/1 98 21) 2,6-Dinitrotoluene 20.77 165 69227 7.08 ug/1 # 82 22) Acenaphthylene 20.74 152 393885 8.02 ug/1 99 23) Acenaphthene 21.31 153 277473 8.08 ug/1 99 24) 2,4-Dinitrotoluene 21.94 165 89884 6.87 ug/.l # 80 25) Diethylphthalate 22.69 149 340971 8.72 ug/1 95 26) 4-Chlorophenyl-phenylether 22.85 204 152308 9.09 ug/1 90 27) Fluorene 22.82 166 314981 8.67 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.31 77 294835 7.03 ug/L # 86

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0308.M Mon Mar 25 09:08:39 2002 Page 1

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