GCMS reference data for sample AE04388, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2502\REF2A.D Vial: 11 Acq On : 25 Mar 2002 8:04 pm Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 28 11:12 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.25 152 479747 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 1837984 20.00 ug/1 -0.11 17) Acenaphthene-diO 21.20 164 999652 20.00 ug/1 -0.12 29) Phenanthrene-diO 25.64 188 1457750 20.00 ug/1 -0.13 38) Chrysene-dl2 33.70 240 851450 20.00 ug/1 -0.15 44) Perylene-dl2 37.94 264 506894 20.00 ug/1 -0.18

System Monitoring Compounds 5.440 37) 2,4-DDD 30.71 235 99732 8.36ug/mL 0.21 Spiked Amount 5.000 Recovery 167.20% /037o Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.90 74 112037 6.88 ug/1 # 68 3) bis(2-Chloroethyl)ether 11.65 93 254698 9.72 ug/1 91 4) 1,3-Dichlorobenzene 12.15 146 102654 3.79 ug/1 97 5) 1,4-Dichlorobenzene 12.30 146 118402 4.36 ug/1 100 6) 1,2-Dichlorobenzene 12.81 146 132998 5.25 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.13 45 342572 9.29 ug/1 99 8) N-Nitroso-di-n-propylamine 13.51 70 177010 10.38 ug/1 # 86 9) Hexachloroethane 13.66 117 16730 1.65 ug/1 98 11) Nitrobenzene 13.93 77 229989 9.15 ug/1 92 12) 1sophorone 14.58 82 523952 11.00 ug/1 100 13) bis(2-Chloroethoxy)methane 15.26 93 313649 10.06 ug/1 97 14) 1,2,4-Trichlorobenzene 15.77 180 117279 5.44 ug/1 94 15) Naphthalene 15.94 128 587871 8.65 ug/1 99 16) Hexachlorobutadiene 16.49 225 10601 0.99 ug/1 100 18) Hexachlorocyclopentadiene 18.68 237 7079 1.05 ug/1 97 19) 2-Chloronaphthalene 19.45 162 367472 8.56 ug/1 95 20) Dimethylphthalate 20.53 163 558932 11.11 ug/1 99 21) 2,6-Dinitrotoluene 20.75 165 121538 9.95 ug/1 # 79 22) Ac enapht hylene 20.72 152 631453 10.29 ug/1 99 23) Acenaphthene 21.29 153 426399 9.94 ug/1 98 24) 2,4-Dinitrotoluene 21.92 165 149154 9.13 ug/1 # 74 25) Diethylphthalate 22.67 149 540143 11.06 ug/1 95 26) 4-Chlorophenyl-phenylether 22.83 204 221483 10.59 ug/1 89 27) Fluorene 22.80 166 481524 10.62 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.29 77 455550 8.70 ug/L # 84

(#) = qualifier out of range (m) = manual integration REF2A.D GCMS0308.M Thu Mar 28 11:13:21 2002 Page 1

NYC-WTC_000011854