GCMS quantitative results for sample AE03823, March 26, 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2202\REF2.D Vial: 5 Acq On : 22 Mar 2002 10:04 pm Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 26 14:25 2002 <Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 371737 20.00 ug/1 -0.09 10) Naphthalene-d8 15.90 136 1455307 20.00 ug/1 -0.10 17) Acenaphthene-diO 21.21 164 789899 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.66 188 1194315 20.00 ug/1 -0.11 38) Chrysene-dl2 33.72 240 776240 20.00 ug/1 -0.13 44) Perylene-dl2 37.97 264 448621 20.00 ug/1 -0.15

System Monitoring Compounds 37) 2,4-DDD 30.73 235 80847 g/mL 0.24 Spiked Amount 5.000 Recovery

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 84602 6.71 ug/1 # 72 3) bis(2-Chloroethyl)ether 11.66 93 198164 9.76 ug/1 91 4) 1,3-Dichlorobenzene 12.16 146 141404 6.74 ug/1 99 5) 1,4-Dichlorobenzene 12.31 146 152753 7.26 ug/1 99 6) 1,2-Dichlorobenzene 12.82 146 158146 8.06 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 13.15 45 278233 9.74 ug/1 99 8) N-Nitroso-di-n-propylamine 13.53 70 136417 10.32 ug/1 # 86 9) Hexachioroethane 13.68 117 33164 4.22 ug/1 98 11) Nitrobenzene 13.94 77 183379 9.22 ug/1 92 12) 1sophorone 14.60 82 404804 10.73 ug/1 98 13) bis(2-Chloroethoxy)methane 15.28 93 243434 9.86 ug/1 99 14) 1,2,4-Trichlorobenzene 15.79 180 138272 8.09 ug/1 94 15) Naphthalene 15.95 128 527514 9.81 ug/1 99 16) Hexachlorobutadiene 16.51 225 25288 2.97 ug/1 96 18) Hexachlorocyclopentadiene 18.70 237 15495 2.90 ug/1 97 19) 2-Chloronaphthalene 19.46 162 323130 9.53 ug/1 98 20) Dimethylphthalate 20.55 163 424740 10.69 ug/1 99 21) 2,6-Dinitrotoluene 20.77 165 89503 9.28 ug/1 # 81 22) Acenaphthylene 20.74 152 510438 10.53 ug/1 99 2 3) Acenaphthene 21.31 153 350158 10.33 ug/1 98 24) 2,4-Dinitrotoluene 21.94 165 114722 8.89 ug/1 # 76 25) Diethylphthalate 22.69 149 417024 10.81 ug/1 95 26) 4-Chlorophenyl-phenylether 22.85 204 186081 11.26 ug/1 90 27) Fluorene 22.82 166 385869 10.77 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.31 77 374580 9.06 ug/L # 87

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0308.M Tue Mar 26 14:29:58 2002 Page 1

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