GCMS reference data for sample AE04388, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2502\REF.D Vial: 10 Acq On : 25 Mar 2002 7:05 pm Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 28 11:08 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 472192 20.00 ug/1 -0.10 10) Naphthalene-d8 15.88 136 1799708 20.00 ug/1 -0.11 17) Acenaphthene-diO 21.19 164 981970 20.00 ug/1 -0.12 29) Phenanthrene-diO 25.63 188 1433698 20.00 ug/1 -0.13 38) Chrysene-dl2 33.70 240 862009 20.00 ug/1 -0.14 44) Perylene-dl2 37.94 264 514786 20.00 ug/1 -0.18

System Monitoring Compounds 37) 2,4-DDD 30.71 235 94691 5.3 , ‘8.047 ug/mL 0.21 Spiked Amount 5.000 Recovery = 181.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.90 74 104651 6.53 ug/1 # 67 3) bis(2-Chloroethyl)ether 11.64 93 246242 9.55 ug/1 90 4) 1,3-Dichlorobenzene 12.15 146 100112 3.76 ug/1 99 5) 1,4-Dichlorobenzene 12.29 146 113184 4.24 ug/1 99 6) 1,2-Dichlorobenzene 12.81 146 129981 5.22 ug/1 99 7) 2,2'-oxybi s(1-Chloropropan 13.13 45 328678 9.05 ug/1 98 8) N-Nitroso-di-n-propylamine 13.52 70 165358 9.85 ug/1 # 86 9) Hexachloroethane 13.66 117 16396 1.64 ug/1 90 11) Nitrobenzene 13.93 77 221801 9.02 ug/1 93 12) 1sophorone 14.58 82 495470 10.62 ug/1 98 13) bis(2-Chloroethoxy)methane 15.26 93 297531 9.74 ug/1 98 14) 1,2,4-Trichlorobenzene 15.77 180 116625 5.52 ug/1 98 15) Naphthalene 15.95 128 569508 8.56 ug/1 99 16) Hexachlorobutadiene 16.49 225 11195 1.06 ug/1 92 18) Hexachlorocyclopentadiene 18.68 237 7240 1.09 ug/1 97 19) 2-Chloronaphthalene 19.45 162 355747 8.44 ug/1 96 20) Dimethylphthalate 20.54 163 528302 10.69 ug/1 99 21) 2,6-Dinitrotoluene 20.75 165 113836 9.49 ug/1 # 81 22) Acenaphthylene 20.72 152 609561 10.11 ug/1 100 23) Acenaphthene 21.28 153 411408 9.77 ug/1 98 24) 2,4-Dinitrotoluene 21.92 165 143642 8.95 ug/1 # 74 25) Diethylphthalate 22.67 149 514671 10.73 ug/1 95 26) 4-Chlorophenyl-phenylether 22.82 204 215189 • 10.48 ug/1 90 27) Fluorene 22.81 166 461731 10.36 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.29 77 427434 8.31 ug/L # 83

(#) = qualifier out of range (m) = manual integration REF.D GCMS0308.M Thu Mar 28 11:09:27 2002 Page 1

NYC-WTC_000011851