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GCMS reference results, Sample AE04417, Mar 2002

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Laboratory report for GC/MS reference analysis of sample AE04417 conducted on March 22, 2002.

NYC-WTC_000012309–000012316

Folder label: “GCMS X 3-1-02 A 3-21-02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR21O2\REF1.D Vial: 4 Acq On : 21 Mar 2002 2:14 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 22 8:42 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.23 168 132003 5.03 ug/1 # 84 31) 4-Bromophenyl-phenylether 24.32 248 87662 5.68 ug/1 # 89 3 2) Hexachiorobenzene 24.75 284 96366 5.38 ug/1 93 3 3) Phenanthrene 25.72 178 507284 6.05 ug/1 98 3 4) Anthracene 25.86 178 454893 5.47 ug/1 98 35) Di-n-butylphthalate 27.62 149 634292 6.01 ug/1 99 3 6) Fluoranthene 29.35 202 494373 5.62 ug/1 # 93 3 9) Pyrene 30.03 202 511079 7.49 ug/1 # 93 40) Butylbenzylphthalate 32.16 149 234762 6.68 ug/1 # 96 41) Benzo(a)anthracene 33.66 228 332781 5.87 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.93 149 310985 6.55 ug/1 95 43) Chrysene 33.79 228 363247 6.53 ug/1 99 45) Di-n-Octylphthalate 35.67 149 399174 6.16 ug/1 # 98 4 6) Benzo(b)fluoranthene 36.78 252 267547 5.95 ug/1 98 47) Benzo(k)fluoranthene 36.84 252 288731 6.59 ug/1 # 97 48) Benzo(a)pyrene 37.77 252 171867 4.20 ug/1 # 95 49) Indeno(l,2,3-cd)pyrene 42.10 276 222955 4.51 ug/1 # 95 50) Dibenz(a,h)anthracene 42.18 278 192859 5.04 ug/1 96 51) Benzo(g,h,i)perylene 43.35 276 189955 4.71 ug/1 96

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0308.M Fri Mar 22 08:52:23 2002 Page 2

NYC-WTC_000012312

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NYC-WTC_000012312Source: NYC Law Department, mirrored locally

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