GCMS calibration results for sample AE04803, April 2002

NYC 9/11 Public Portal Document

Quantitation Repqrt (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR2 8 02\ 25., Vial: 2 Acq On 28 Mar 2002 9:30 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 9:41 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth-: GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 612785 20.00 ug/1 -0.09 10) Naphthalene-d8 15.89 136 2660921 20.00 ug/1 -0.10 17) Acenaphthene-dlO 21.20 164 1486283 20.00 ug/1 -0.11 29) Phenanthrene-dlO 25.64 188 2226728 20.00 ug/1 -0.12 38) Chrysene-dl2 33.71 240 1317395 20.00 ug/1 -0.13 44) Perylene-dl2 37.95 264 688093 20.00 ug/1 -0.18

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = ^00%

Target Compounds 2) N-nitroso-dimethyl amine 5.89 74 480796 23.13 ug/1 # 70 3) bis(2-Chloroethyl)ether 11.66 93 907780 27.12 ug/1 92 4) 1,3-Dichlorobenzene 12.16 146 873743 25.26 ug/1 100 5) 1,4-Dichlorobenzene 12.30 146 894648 25.80 ug/1 99 6) 1,2-Dichlorobenzene 12.82 146 849848 26.28 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 13.13 45 1231902 26.15 ug/1 99 8) N-Nitroso-di-n-propylamine 13.54 70 603563 27.71 ug/1 # 87 9) Hexachloroethane 13.66 117 329746 25.44 ug/1 . 94 11) Nitrobenzene 13.95 77 893392 24.56 ug/1 91 12) Isophorone 14.59 82 1704982 24.71 ug/1 99 13) bis(2-Chloroethoxy)methane 15.27 93 1127463 24.97 ug/1 98 14) 1,2,4-Trichlorobenzene 15.78 180 832053 26.64 ug/1 96 15) Naphthalene 15.95 128 2585123 26.28 ug/1 99 16) Hexachlorobutadiene 16.49 225 429481 27.58 ug/1 99 18) Hexachlorocyclopentadiene 18.69 237 269198 26.74 ug/1 99 19) 2-Chloronaphthalene 19.46 162 1619665 25.38 ug/1 97 20) Dimethylphthalate 20.55 163 1877911 25.11 ug/1 99 21) 2,6-Dinitrotoluene 20.77 165 449617 24.77 ug/1 # 81 22) Acenaphthylene 20.73 152 2308362 25.30 ug/1 99 23) Acenaphthene 21.30 153 1621062 25.42 ug/1 98 24) 2,4-Dinitrotoluene 21.94 165 577910 23.79 ug/1 # 79 25) Diethylphthalate 22.69 149 1802994 24.83 ug/1 96 26) 4-Chlorophenyl-phenylether 22.83 204 836990 26.92 ug/1 91 27) Fluorene 22.82 166 1753502 26.00 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.30 77 1713129 22.01 ug/L # 85

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS0308.M Mon Apr 01 14:51:40 2002 Page 1

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