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GCMS calibration results for sample AE04803, April 2002

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Laboratory report listing concentrations of target analytes in a reference standard analyzed on April 2, 2002.

NYC-WTC_000058494–000058497

Folder label: “GCMS X 3/5/02 A 3/29/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2802\CAL25.D Vial: 2 Acq On : 28 Mar 2002 . 9:30 am Operator : Sample : Inst : GC/MS 209 ' Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 9:41 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.24 168 734787 24.43 ug/1 # 80 31) 4-Bromophenyl-phenylether 24.30 248 467088 26.42 ug/1 # 91 32) Hexachlorobenzene 24.74 284 549079 26.75 ug/1 92 33) Phenanthrene 25.72 178 2414490 25.11 ug/1 99 ■ 34) Anthracene 25.85 178 2209455 23.16 ug/1 99 35) Di-n-butylphthalate 27.61 149 2994735 24.74 ug/1 99 36) Fluoranthene 29.34 202 2456245 24.34 ug/1 96 39) Pyrene 30.01 202 2449797 32.39 ug/1 # 92 40) Butylbenzylphthalate 32.14 149 1129659 28.96 ug/1 # 96 41) Benzo(a)anthracene 33.65 228 1537987 24.45 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.92 149 1371152 26.04 ug/1 95 43) Chrysene 33.79 228 1532430 24.84 ug/1 99 45) Di-n-Octylphthalate 35.66 149 1910084 31.50 ug/1 # 96 46) Benzo(b)fluoranthene 36.76 252 1.183649m 28.17 ug/1 47) Benzo(k)fluoranthene 36.83 252 1214692 29.65 ug/1 97 48) Benzo(a)pyrene 37.75 252 907951 23.71 ug/1 # 97 49) Indeno(1,2,3-cd)pyrene 42.09 276 888690 19.22 ug/1 96 50) Dibenz(a,h)anthracene 42.15 278 680504 19.01 ug/1 96 51) Benzo(g,h,i)perylene 43.33 276 724286 19.20 ug/1 96

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(#) = qualifier out of range (m) = manual integration CAL25.D GCMS0308.M Mon Apr 01 14:51:43 2002 Page 2

NYC-WTC_000058496

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NYC-WTC_000058496Source: NYC Law Department, mirrored locally

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