Calibration log listing response factors for nitrosamines and chlorinated solvents on March 29, 2002.
NYC-WTC_000058171–000058174Folder label: “GCMS X 3/2/02 A 3/27/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAR2702\CAL40.D Vial: 2 Acq On : 27 Mar 2002 2:38 pm Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 29 12:24 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 23.25 168 1307141 39.14 ug/1 # 83 31) 4-Bromophenyl-phenylether 24.31 248 819827 41.77 ug/1 # 89 3 2) Hexachlorobenzene 24.75 284 963790 42.29 ug/1 # 88 33) Phenanthrene 25.73 178 4200741 39.34 ug/1 99 34) Anthracene 25.86 178 4069296 38.42 ug/1 99 35) Di-n-butylphthalate 27.63 149 5173212 38.49 ug/1 # 98 3 6) Fluoranthene 29.35 202 4284040 38.24 ug/1 # 93 3 9) Pyrene 30.03 202 4309824 50.71 ug/1 # 94 40) Butylbenzylphthalate 32.15 149 2018456 46.06 ug/1 96 41) Benzo(a)anthracene 33.67 228 2775255 39.26 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.92 149 2417010 40.85 ug/1 # 95 43) Chrysene 33.80 228 2698089 38.93 ug/1 99 45) Di-n-Octylphthalate 35.66 149 3445906 49.24 ug/1 # 97 46) Benzo(b)fluoranthene 36.78 252 2254455 46.49 ug/1 98 47) Benzo(k)fluoranthene 36.85 252 2189864 46.31 ug/1 98 4 8) Benzo(a)pyrene 37.77 252 1744109 39.46 ug/1 # 97 49) Indeno(l,2,3-cd)pyrene 42.10 276 1659852 31.10 ug/1 96 5 0) Dibenz(a,h)anthracene 42.18 278 1273249 30.82 ug/1 97 51) Benzo(g,h,i)perylene 43.36 276 1319096 30.30 ug/1 97
(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0308.M Fri Mar 29 12:27:18 2002 Page 2
NYC-WTC_000058173
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NYC-WTC_000059218
Calibration data for gas chromatography mass spectrometry analysis of volatile organic compounds dated April 4, 2002.
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Laboratory report showing GCMS calibration analysis for volatile organic compounds on March 29, 2002.
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Calibration results for specific volatile organic compounds used to verify GCMS instrument performance in April 2002.
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Laboratory report listing concentrations of target analytes in a reference standard analyzed on April 2, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058258
Reference standard analysis report for sample AE04733 conducted April 1, 2002, listing concentrations of quality control compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059487
Laboratory report of a GCMS blank test conducted on April 5, 2002, showing non-detect levels for various organic compounds.
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Laboratory report showing GCMS blank analysis for volatile organic compounds on April 2, 2002.
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Laboratory report for GC/MS calibration analysis of sample AE04417 conducted on March 22, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010285
Calibration table listing response factors and retention times for standard compounds used to verify instrument performance on March 21, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011707
Laboratory report of a GCMS blank run on March 27, 2002, listing target compounds and detection limits.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011074
Calibration data report for sample AE03075 dated March 5, 2002, showing response values.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012309
Laboratory report for GC/MS reference analysis of sample AE04417 conducted on March 22, 2002.
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NYC-WTC_000058159
Unreadable text fragment containing a file identifier from the March 2002 GCMS batch records.
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NYC-WTC_000058160
Fragmented text containing a unique file identifier from the March 2002 GCMS batch records.
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NYC-WTC_000058163
Laboratory blank analysis report showing all target compounds detected below the method detection limit on March 29, 2002.
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NYC-WTC_000058175
Analysis of reference standards for nitrosamines and VOCs with measured concentrations near target levels on March 29, 2002.
Filed in the same folder
NYC-WTC_000058183
GCMS analysis of sample AE04416 for organic compounds with surrogate standard showing 5.0 micrograms detection limit.
Filed in the same folder