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GCMS calibration results, sample AE05234, April 2002

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Calibration results for specific volatile organic compounds used to verify GCMS instrument performance in April 2002.

NYC-WTC_000059114–000059117

Folder label: “GCMS X 3/9/02 A 3/30/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File ; C:\HPCHEM\l\DATA\MAR3002\CAL40A.D Vial: 2 Acq On 30 Mar 2002 4:46 pm Operator : Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 2 15:08 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.25 168 1475567 38.64 ug/1 # 83 31) 4-Bromophenyl-phenylether 24.31 248 909778 40.54 ug/1 # 90 32) Hexachlorobenzene 24.75 284 1071363 41.12 ug/1 # 87 33) Phenanthrene 25.73 178 4629333 37.92 ug/1 99 34) Anthracene 25.86 178 4520103 37.33 ug/1 99 35) Di-n-butylphthalate 27.62 149 5677125 36.95 ug/1 99 36) Fluoranthene 29.35 202 4675742 36.51 ug/1 # 94 39) Pyrene 30.03 202 4690002 49.42 ug/1 93 40) Butylbenzylphthalate 32.15 149 2086570 42.64 ug/1 96 41) Benzo(a)anthracene 33.67 228 3000421 38.01 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.92 149 2410073 36.48 ug/1 # 94 43) Chrysene 33.81 228 2882858 37.24 ug/1 99 45) Di-n-Octylphthalate 35.66 149 3419141 44.33 ug/1 # 97 46) Benzo(b)fluoranthene 36.78 252 2379542 44.52 ug/1 98 47) Benzo(k)fluoranthene 36.85 252 2312464m 44.37 ug/1 48) Benzo(a)pyrene 37.77 252 1849908 37.97 ug/1 # 97 49) Indeno(1,2,3-cd)pyrene 42.10 276 1786081 30.36 ug/1 96 50) Dibenz(a,h)anthracene 42.17 278 1387660 30.47 ug/1 97 51) Benzo(g,h,i)perylene 43.36 276 1431096 29.82 ug/1 97

{#) = qualifier out of range (m) = manual integration CAL40A.D GCMS0308.M Wed Apr 03 13:32:16 2002 Page 2

NYC-WTC_000059116

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NYC-WTC_000059116Source: NYC Law Department, mirrored locally

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