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GCMS calibration results for sample AE03075, March 5 2002

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Calibration data report for sample AE03075 dated March 5, 2002, showing response values.

NYC-WTC_000011074–000011077

Folder label: “GCMS X 2/12/02 A 3/19/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR010 2\CALI0A.D Vial: 2 Acq On 2 Mar 2002 7:56 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 5 12:41 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.30 168 386728 19.2 g/1 # 86 31) 4-Bromophenyl-phenylether 24.37 248 95871 .3 ug/1 95 32) Hexachlorobenzene 24.80 284 112063 7.36 ug/1 98 33) Phenanthrene 25.79 178 519817 8.38 ug/1 100 34) Anthracene 25.91 178 524800 8.63 ug/1 100 35) Di-n-butylphthalate 27.68 149 671771 7.75 ug/1 99 36) Fluoranthene 29.41 202 526657 8.50 ug/1 # 92 3 9) Pyrene 30.08 202 539864 8.46 ug/1 # 87 40) Butylbenzylphthalate 32.21 149 276227 7.81 ug/1 97 41) Benzo(a)anthracene 33.73 228 383061 8.21 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.98 149 352805 7.39 ug/1 96 43) Chrysene 33.86 228 382047 8.32 ug/1 100 45) Di-n-Octylphthalate 35.73 149 508104 6.72 ug/1 # 98 46) Benzo(b)fluoranthene 36.85 252 339031 7.94 ug/1 # 97 47) Benzo(k)fluoranthene 36.91 252 380930 8.88 ug/1 # 92 48) Benzo(a)pyrene 37.85 252 284984 8.06 ug/1 # 94 49) Indeno(1,2,3-cd)pyrene 42.24 276 287265 8.90 ug/1 # 93 50) Dibenz(a,h)anthracene 42.31 278 217523 8.82 ug/1 # 93 51) Benzo(g,h,i)perylene 43.50 276 236791 9.10 ug/1 95

(#) = qualifier out of range (m) = manual integration CAL10A.D GCMS0208.M Tue Mar 05 13:56:17 2002 Page 2

NYC-WTC_000011076

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NYC-WTC_000011076Source: NYC Law Department, mirrored locally

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