GCMS calibration results for sample AE03075, March 5 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR0102\CAL10A.D Vial: 2 Acq On 2 Mar 2002 7:56 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 5 12:41 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.32 152 324020 20.00 ug/1 -0.03 10) Naphthalene-d8 15.95 136 1272671 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.27 164 688021 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.72 188 1026100 20.00 ug/1 -0.04 38) Chrysene-dl2 33.78 240 729066 20.00 ug/1 -0.06 44) Perylene-dl2 38.05 264 472221 20.00 ug/1 -0.07

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue . 2) N-nitroso-dimethyl amine 5.93 74 133957 10.33 ug/1 # 73 3) bis(2-Chloroethyl)ether 11.72 93 213582 10.03 ug/1 92 4) 1,3-Dichlorobenzene 12.22 146 218252 8.61 ug/1 100 5) 1,4-Dichlorobenzene 12.36 146 220596 8.54 ug/1 99 6) 1,2-Dichlorobenzene 12.88 146 205574 8.37 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.19 45 303989 9.43 ug/1 99 8) N-Nitroso-di-n-propylamine 13.59 70 141671 9.30 ug/1 94 9) Hexachloroethane 13.72 117 82786 8.00 ug/1 95 11) Nitrobenzene 14.00 77 209945 8.02 ug/1 96 12) Isophorone 14.65 82 393292 8.90 ug/1 99 13) bis(2-Chloroethoxy)methane 15.33 93 327643 11.90 ug/1 99 14) 1,2,4-Trichlorobenzene 15.84 180 177229 8.14 ug/1 95 15) Naphthalene 16.01 128 582155 8.59 ug/1 99 16) Hexachlorobutadiene 16.56 225 91688 7.03 ug/1 99 18) Hexachlorocyclopentadiene 18.75 237 64575 6.5 g/l 99 19) 2-Chloronaphthalene 19.53 162 373901 9.11 ug/1 97 20) Dimethylphthalate 20.61 163 397098 8.31 ug/1 100 21) 2,6-Dinitrotoluene 20.83 165 94730 8.75 ug/1 # 83 22) Acenaphthylene 20.80 152 504551 8.51 ug/1 99 2 3) Acenaphthene 21.36 153 355854 8.59 ug/1 99 24) 2,4-Dinitrotoluene 21.99 165 120000 8.75 ug/1 # 85 25) Diethylphthalate 22.75 149 389979 7.85 ug/1 97 26) 4-Chlorophenyl-phenylether 22.90 204 175966 8.23 ug/1 93 27) Fluorene 22.89 166 381585 8.44 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 23.37 77 408679 7.83 ug/L # 87

(#) = qualifier out of range (m) = manual integration CAL10A.D GCMS0208.M Tue Mar 05 13:56:13 2002 Page 1

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