GCMS calibration data for organic compounds, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAR1902\C 10. .D Vial: 2 Acq On 20 Mar 2002 12:06 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 21 8:21 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.27 152 563664 20.00 ug/1 -0.08 10) Naphthalene-d8 15.91 136 2204892 20.00 ug/1 -0.09 17) Acenaphthene-diO 21.22 164 1196644 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.66 188 1845176 20.00 ug/1 -0.11 38) Chrysene-dl2 33.73 240 1295212 20.00 ug/1 -0.12 44) Perylene-dl2 37.98 264 866312 20.00 ug/1 -0.14

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds 2) N-nitroso-dimethyl amine 5.91 74 204774 1-V Qvalue 10.71 ug/1 # 69 3) bis(2-Chloroethyl)ether 11.68 93 336778 10.94 ug/1 91 4) 1,3-Dichlorobenzene 12.17 146 350626 11.02 ug/1 99 5) 1,4-Dichlorobenzene 12.31 146 350941 11.00 ug/1 99 6) 1,2-Dichlorobenzene 12.83 146 328874 11.06 ug/1 99 7) 2,2'-oxybis(1-Chicropropan 13.15 45 456900 10.54 ug/1 99 8) N-Nitroso-di-n-propylamine 13.54 70 219561 10.96 ug/1 # 86 9) Hexachloroethane 13.68 117 130532 10.95 ug/1 99 11.) Nitrobenzene 13.95 77 325106 10.79 ug/1 93 12) Isophorone 14.60 82 605386 10.59 ug/1 99 13) bis(2-Chloroethoxy)methane 15.28 93 407493 10.89 ug/1 97 14) 1,2,4-Trichlorobenzene 15.79 180 286112 11.05 ug/1 98 15) Naphthalene 15.96 128 921248 11.30 ug/1 99 16) Hexachlorobutadiene 16.51 225 145348 11.26 ug/1 99 18) Hexachlorocyclopentadiene 18.70 237 90386 11.15 ug/1 100 19) 2-Chloronaphthalene 19.47 162 560347 10.91 ug/1 97 20) Dimethylphthalate 20.55 163 651609 10.82 ug/1 99 21) 2,6-Dinitrotoluene 20.77 165 151241 10.35 ug/1 # 82 22) Acenaphthylene 20.74 152 817547 11.13 ug/1 98 2 3) Acenaphthene 21.31 153 572273 11.15 ug/1 98 24) 2,4-Dinitrotoluene 21.94 165 196843 10.07 ug/1 # 78 25) Diethylphthalate 22.69 149 632351 10.82 ug/1 95 26) 4-Chlorophenyl-phenylether 22.85 204 300444 12.00 ug/1 91 27) Fluorene 22.82 166 628313 11.57 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.32 77 641697 10.24 ug/L # 84

(#) = qualifier out of range (m) = manual integration CAL10A.D GCMS0308.M Thu Mar 21 08:26:01 2002 Page 1

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