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GCMS calibration data for organic compounds, March 2002

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Calibration table listing response factors and retention times for standard compounds used to verify instrument performance on March 21, 2002.

NYC-WTC_000010285–000010288

Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) «

Data File C:\HPCHEM\1\DATA\MAR19 02\CAL10A.D Vial: 2 Acq On 20 Mar 2002 12:06 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 21 8:21 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.24 168 261996 10.51 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.32 248 160039 10.93 ug/1 # 90 32) Hexachlorobenzene 24.75 284 185744 10.92 ug/1 92 3 3) Phenanthrene 25.72 178 878387 11.02 ug/1 99 3 4) Anthracene 25.86 178 856621 10.84 ug/1 99 35) Di-n-butylphthalate 27.62 149 1087903 10.85 ug/1 # 98 3 6) Fluoranthene 29.35 202 894425 10.70 ug/1 # 92 3 9) Pyrene 30.03 202 909909 12.23 ug/1 # 92 40) Butylbenzylphthalate 32.15 149 442133 11.53 ug/1 95 41) Benzo(a)anthracene 33.66 228 650482 10.52 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.93 149 592586 11.45 ug/1 96 43) Chrysene 33.79 228 652080 10.75 ug/1 99 45) Di-n-Octylphthalate 35.67 149 910752 11.93 ug/1 # 99 46) Benzo(b)fluoranthene 36.78 252 548882 10.38 ug/1 # 97 47) Benzo(k)fluoranthene 36.84 252 580303 11.25 ug/1 # 96 4 8) Benzo(a)pyrene 37.78 252 491412 10.19 ug/1 # 95 49) Indeno(l,2,3-cd)pyrene 42.11 276 506940 8.71 ug/1 95 50) Dibenz(a,h)anthracene 42.18 278 391277 8.68 ug/1 # 95 51) Benzo(g,h,i)perylene 43.36 276 422281 8.89 ug/1 # 93

(#) = qualifier out of range (m) = manual integration CAL10A.D GCMS0308.M Thu Mar 21 08:26:05 2002 Page 2

NYC-WTC_000010287

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