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GCMS calibration data for sample AE03265, March 2002

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Laboratory report documenting GCMS calibration results for environmental sample AE03265 conducted on March 25, 2002.

NYC-WTC_000011377–000011379

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR0102\CAL1 .D Vial: 2 Acq On : 2 Mar 2002 10:42 pm — Operator: / Sample : Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 25 11:56 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

3 0) N-Nitrosodiphenylamine 23.30 168 405157 19.25 ug/1 # 84 31) 4-Bromophenyl-phenylether 24.38 248 100700 7.40 ug/1 92 32) Hexachlorobenzene 24.81 284 116812 7.33 ug/1 96 33) Phenanthrene 2 5.79 178 542244 8.35 ug/1 99 34) Anthracene 25.92 178 547206 8.60 ug/1 99 35) Di -n-butylphthalate 27.68 149 700090 7.72 ug/1 98 36) Fluoranthene 2 9.41 202 556039 8.58 ug/1 # 89 3 9) Pyrene 30.09 202 568250 8.20 ug/1 # 88 40) Butylbenzylphthalate 32.22 149 289273 7.53 ug/1 99 41) Benzo(a)anthracene 33.73 228 420346 8.29 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.99 149 363971 7.02 ug/1 95 43) Chrysene 33.86 228 407042 8.16 ug/1 99 45) Di-n-Octylphthalate 3 5.73 14 9 526612 6.47^9/1 # 98 46) Benzo(b)fluoranthene 36.85 252 375669 8-18 ug/1 # 97 47) Benzo(k)fluoranthene 36.92 252 401482 8.69 ug/1 # 93 48) Benzo(a)pyrene 37.85 252 310947 8.16 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.24 276 305771 8.80 ug/1 # 94 50) Dibenz(a,h)anthracene 42.31 278 239367 9.01 ug/1 # 94 51) Benzo(g,h,i)perylene 43.50 276 248568 8.87 ug/1 # 93

(#) = qualifier out of range (m) = manual integration CALIOB.D GCMS0208.M Mon Mar 25 11:59:27 2002 Page 2

NYC-WTC_000011378

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NYC-WTC_000011378Source: NYC Law Department, mirrored locally

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