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GCMS analysis results for sample AE02595, Mar 2002

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Laboratory report detailing GCMS detection of volatile organic compounds in sample AE02595 conducted on March 4, 2002.

NYC-WTC_000005243–000005246

Folder label: “GCMS X 2/5/02 A 3/1/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR0102\CAL10.D Vial: 2 Acq On 1 Mar 2002 9:20 am Operator: Sample Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 1 14:20 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.30 168 351835 19.14 ug/1 # 87 31) 4-Bromophenyl-phenylether 24.37 248 87824 /7 .39ug/1 95 32) Hexachlorobenzene 24.81 284 101861 7.32/ug/1 95 33) Phenanthrene 25.78 178 474601 8.37 ug/1 99 34) Anthracene 25.91 178 475372 8.56 ug/1 99 35) Di-n-butylphthalate '27.68 149 612692 (7.73 ug/1 99 36) Fluoranthene 29.41 202 478413 8.45 ug/1 # 90 3 9) Pyrene 30.09 202 492949 8.27 ug/1 # 90 40) Butylbenzylphthalate 32.21 149 251169 (7.61 ug/1 97 41) Benzo(a)anthracene 33.72 228 359639 8.25 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.99 149 318960 (7.15 ug/1 96 43) Chrysene 33.85 228 352146 8.21 ug/1 99 45) Di-n-Octylphthalate 35.73 149 454192 (6.38 ug/1 99 46) Benzo(b)fluoranthene 36.85 252 287917 (7.17 ug/1 # 96 47) Benzo(k)fluoranthene 36.92 252 347678 8.61 ug/1 # 94 48) Benzo(a)pyrene 37.86- 252 271071 8.14 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.24 276 271231 8.92 ug/1 95 50) Dibenz(a,h)anthracene 42.32 278 211300 9.10 ug/1 # 95 51) Benzo(g,h,i)perylene 43.50 276 221219 9.03 ug/1 94

(#) = qualifier out of range (m) = manual integration CALIO . D GCMS0208.M Mon Mar 04 10:40:14 2002 Page 2

NYC-WTC_000005245

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NYC-WTC_000005245Source: NYC Law Department, mirrored locally

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