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GCMS analysis results for sample AE02595, Mar 2002

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Laboratory report detailing GCMS detection of volatile organic compounds in sample AE02595 conducted on March 4, 2002.

NYC-WTC_000005247–000005251

Folder label: “GCMS X 2/5/02 A 3/1/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR0102\REF.D Vial: 4 Acq On 1 Mar 2002 11:17 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 4 10:44 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.29 168 46522 2.89 ug/1 # 86 31) 4-Bromophenyl-phenylether 24.37 248 30003 2.89 ug/1 93 32) Hexachlorobenzene 24.80 284 33189 2.73 ug/1 97 33) Phenanthrene 25.78 178 177624 3.58 ug/1 98 34) Anthracene 25.91 178 156817 3.23 ug/1 98 35) Di-n-butylphthalate 27.68 149 237519 3.43 ug/1 99 36) Fluoranthene 29.41 202 172169 3.48 ug/1 # 92 3 9) Pyrene 30.08 202 177902 3.55 ug/1 # 86 40) Butylbenzylphthalate 32.21 149 79952 2.88 ug/1 97 41) Benzo(a)anthracene 33.73 228 134160 3.66 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.99 149 122534 3.27 ug/1 98 43) Chrysene 33.85 228 143328 3.97 ug/1 99 45) Di-n-Octylphthalate 35.73 149 152593 2.42 ug/1 # 97 46) Benzo(b)fluoranthene 36.85 252 121201 3.41 ug/1 # 97 47) Benzo(k)fluoranthene 36.91 252 134207 3.76 ug/1 # 95 48) Benzo(a)pyrene 37.85. 252 87750 2.98 ug/1 # 93 49) Indeno(1,2,3-cd)pyrene 42.24 276 99325 3.70 ug/1 # 91 50) Dibenz(a,h)anthracene 42.31 278 85669 4.17 ug/1 # 93 51) Benzo(g,h,i)perylene 43.49 276 91096 4.20 ug/1 # 93

(#) = qualifier out of range (m) = manual integration REF.D GCMS0208.M Mon Mar 04 10:46:52 2002 Page 2

NYC-WTC_000005250

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NYC-WTC_000005250Source: NYC Law Department, mirrored locally

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