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GCMS reference analysis results for sample AE03265, March 2002

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Laboratory report documenting GCMS reference analysis of sample AE03265 conducted on March 25, 2002.

NYC-WTC_000011388–000011395

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MARO1O2\REFC2 .D Vial: 39 Acq On 3 Mar 2002 1:40 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 6 10:40 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.29 168 87415 5.98 ug/1 # 84 31) 4-Bromophenyl-phenylether 24.37 248 65542 6.94 ug/1 95 32) Hexachlorobenzene 24.81 284 78981 7.14 ug/1 # 92 3 3) Phenanthrene 25.78 178 366582 8.14 ug/1 99 34) Anthracene 25.91 178 338563 7.67 ug/1 99 35) Di-n-butylphthalate 27.68 149 478909 7.61 ug/1 99 36) Fluoranthene 29.41 202 359840 8.00 ug/1 # 90 3 9) Pyrene 30.09 202 374426 8.57 ug/1 # 90 40) Butylbenzylphthalate 32.21 149 164213 6.78 ug/1 94 41) Benzo(a)anthracene 33.73 228 259816 8.13 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.99 149 248557 7.60 ug/1 96 43) Chrysene 33.85 228 277401 8.82 ug/1 100 45) Di-n-Octylphthalate 35.73 149 306865 5.84 ug/1 99 46) Benzo(b)fluoranthene 36.85 252 229289 7.74 ug/1 98 47) Benzo(k)fluoranthene 36.91 252 259204 8.70 ug/1 # 95 48) Benzo(a)pyrene 37.85 252 163641 6.66 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.24 276 176989 7.89 ug/1 # 93 50) Dibenz(a,h)anthracene 42.32 278 156519 9.14 ug/1 96 51) Benzo(g,h,i)perylene 43.49 276 160387 8.87 ug/1 # 93

(#) = qualifier out of range (m) = manual integration REFC2.D GCMS0208.M Mon Mar 25 12:01:30 2002 Page 2

NYC-WTC_000011394

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NYC-WTC_000011394Source: NYC Law Department, mirrored locally

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