GCMS reference results for sample AE02581, Mar 13, 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MARO7O2\REF.D Vial: 16 Acq On 8 Mar 2002 4:29 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 8 8:58 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.26 168 61216 2.27 ug/1 # 83 31) 4-Bromophenyl-phenylether 24.35 248 42141 2.42 ug/1 93 32) Hexachlorobenzene 24.78 284 46724 2.29 ug/1 96 3 3) Phenanthrene 25.75 178 249681 3.01 ug/1 98 34) Anthracene 25.89 178 232279 2.86 ug/1 99 35) Di-n-butylphthalate 27.65 149 327904 2.83 ug/1 98 36) Fluoranthene 29.38 202 251166 3.03 ug/1 # 89 3 9) Pyrene 30.06 202 265338 2.68 ug/1 # 89 40) Butylbenzylphthalate 32.19 149 110032 2.01 ug/1 97 41) Benzo(a)anthracene 33.70 228 218007 3.01 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.97 149 181987 2.46 ug/1 96 43) Chrysene 33.83 228 238930 3.35 ug/1 99 45) Di-n-Octylphthalate 35.70 149 229781 1.70 ug/1 99 46) Benzo(b)fluoranthene 36.81 252 190595 2.50 ug/1 # 97 47) Benzo(k)fluoranthene 36.88 252 223589 2.92 ug/1 # 94 48) Benzo(a)pyrene 37.82 252 150482 2.38 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.18 276 170711 2.96 ug/1 # 93 50) Dibenz(a,h)anthracene 42.25 278 150252 3.41 ug/1 # 95 51) Benzo(g,h,i)perylene 43.42 276 150733 3.24 ug/1 # 93

(#) = qualifier out of range (m) = manual integration REF.D GCMS0208.M Wed Mar 13 14:21:07 2002 Page 2

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