GCMS calibration table for TCLP analysis, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR0102\REF1.D Vial: 25 Acq On 2 Mar 2002 9:54 am Operator : Sample gc/ms scan 2/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 5 14:00 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.29 168 111998 3.46 ug/1 # 85 31) 4-Bromophenyl-phenylether 24.37 248 77068 3.68 ug/1 93 32) Hexachlorobenzene 24.81 284 91062 3.72 ug/1 97 3 3) Phenanthrene 25.78 178 440950 4.42 ug/1 99 3 4) Anthracene 25.92 178 404524 4.14 ug/1 99 35) Di-n-butylphthalate 27.68 149 578379 4.15 ug/1 99 36) Fluoranthene 29.41 202 440613 4.42 ug/1 # 93 3 9) Pyrene 30.08 202 457474 4.48 ug/1 # 88 40) Butylbenzylphthalate 32.21 149 203850 3.61 ug/1 97 41) Benzo(a)anthracene 33.73 228 341584 4.58 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.99 149 308046 4.03 ug/1 97 43) Chrysene 33.86 228 361609 4.92 ug/1 99 45) Di-n-Octylphthalate 35.73 149 402265 3.20 ug/1 # 98 46) Benzo(b)fluoranthene 36.85 252 313787 4.42 ug/1 # 97 4 7) Benzo(k)fluoranthene 36.91 252 338081 4.74 ug/1 # 97 48) Benzo(a)pyrene 37.85 252 224792 3.82 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.24 276 254130 4.73 ug/1 # 94 5 0) Dibenz(a,h)anthracene 42.31. 278 223986 5.45 ug/1 # 94 51) Benzo(g,h,i)perylene 43.50 276 224614 5.18 ug/1 # 93

+) = qualifier out of range (m) = manual integration F1.D GCMS0208.M Tue Mar 05 14:03:52 2002 Page 2

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