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GCMS reference standard results, February 2002

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Laboratory report of GCMS analysis of reference standards on February 28, 2002, verifying instrument performance.

NYC-WTC_000010162–000010166

Folder label: “GCMS X 1/25/02 A 2/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB2502\REF.D Vial: 4 Acq On : 25 Feb 2002 1:38 pm Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 28 9:01 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.29 168 33979 2.42 ug/1 # 85 31) 4-Bromophenyl-phenylether 24.37 248 25587 2.82 ug/1 91 32) Hexachlorobenzene 24.80 284 32047 3.01 ug/1 94 3 3) Phenanthrene 25.78 178 144313 3.33 ug/1 99 34) Anthracene 25.91 178 122861 2.89 ug/1 98 35) Di-n-butylphthalate 27.68 149 210631 3.48 ug/1 99 3 6) Fluoranthene 29.40 202 130406 3.01 ug/1 # 89 39) Pyrene 30.08 202 135536 3.49 ug/1 # 88 40) Butylbenzylphthalate 32.21 149 50660 2.36 ug/1 98 41) Benzo(a)anthracene 33.73 228 85407 3.01 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.98 149 78755 2.71 ug/1 96 43) Chrysene 33.85 228 101571 3.63 ug/1 99 45) Di-n-Octylphthalate 35.73 149 74222 1.57 ug/1 # 97 46) Benzo(b)fluoranthene 36.84 252 67872 2.55 ug/1 96 47) Benzo(k)fluoranthene 36.91 252 90484 3.38 ug/1 # 96 4 8) Benzo(a)pyrene 37.85 252 50875 2.30 ug/1 # 95 49) Indeno(l,2,3-cd)pyrene 42.24 276 58958 2.93 ug/1 # 94 50) Dibenz(a,h)anthracene 42.30 278 50669 3.29 ug/1 96 51) Benzo(g,h,i)perylene 43.49 276 57951 3.57 ug/1 # 93

(#) = qualifier out of range (m) = manual integration REF.D GCMS0208.M Thu Feb 28 09:04:12 2002 Page 2

NYC-WTC_000010165

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NYC-WTC_000010165Source: NYC Law Department, mirrored locally

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