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GCMS calibration table for TCLP analysis, March 2002

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Calibration table listing retention times and concentrations for TCLP method analysis in March 2002.

NYC-WTC_000011080–000011082

Folder label: “GCMS X 2/12/02 A 3/19/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAR0102\REF2.D Vial: 26 Acq On 2 Mar 2002 10:53 am Operator: Sample gc/ms scan 2/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 5 14:04 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.29 168 107998 3.40 ug/1 # 87 31) 4-Bromophenyl-phenylether 24.37 248 78689 3.84 ug/1 96 32) Hexachlorobenzene 24.81 284 92130 3.83 ug/1 95 3 3) Phenanthrene 25.78 178 441744 4.51 ug/1 99 34) Anthracene 25.91 178 409486 4.27 ug/1 99 35) Di-n-butylphthalate 27.68 149 593125 4.33 ug/1 99 36) Fluoranthene 29.41 202 448496 4.59 ug/1 # 90 39) Pyrene 30.09 202 463502 4.65 ug/1 # 90 40) Butylbenzylphthalate 32.21 149 207887 3.77 ug/1 96 41) Benzo(a)anthracene 33.73 228 345704 4.74 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.99 149 311369 4.17 ug/1 96 43) Chrysene 33.86 228 361253 5.04 ug/1 100 45) Di-n-Octylphthalate 35.73 149 406066 3.36 ug/1 99 46) Benzo(b)fluoranthene 36.85 252 304878 4.47 ug/1 # 97 47) Benzo(k)fluoranthene 36.91 252 342285 4.99 ug/1 # 96 48) Benzo(a)pyrene 37.86 252 223998 3.96 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 42.24 276 255224 4.94 ug/1 # 95 50) Dibenz(a,h)anthracene 42.32 278 226172 5.73 ug/1 # 96 51) Benzo(g,h,i)perylene 43.49 276 225989 5.43 ug/1 94

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0208.M Tue Mar 05 14:07:23 2002 Page 2

NYC-WTC_000011081

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NYC-WTC_000011081Source: NYC Law Department, mirrored locally

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