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GCMS reference analysis results for sample AE03265, March 2002

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Laboratory report documenting GCMS reference analysis of sample AE03265 conducted on March 25, 2002.

NYC-WTC_000011388–000011395

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR0102\REFC.D Vial: 38 Acq On 3 Mar 2002 12:41 am Operator : Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 6 10:28 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.29 168 91298 5.70 ug/1 # 83 31) 4-Bromophenyl-phenylether 24.37 248 70913 6.85 ug/1 95 3 2) Hexachlorobenzene 24.81 284 84386 6.96 ug/1 95 3 3) Phenanthrene 25.78 178 400596 8.11 ug/1 99 3 4) Anthracene 25.91 178 366786 7.58 ug/1 98 35) Di-n-butylphthalate 27.68 149 531642 7.70 ug/1 99 36) Fluoranthene 29.41 202 402798 8.17 ug/1 # 90 39) Pyrene 30.09 202 418064 8.25 ug/1 # 88 40) Butylbenzylphthalate 32.21 149 186236 6.64 ug/1 94 41) Benzo(a)anthracene 33.73 228 306094 8.26 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.99 149 277665 7.33 ug/1 96 43) Chrysene 33.85 228 322359 8.84 ug/1 98 45) Di-n-Octylphthalate 35.73 149 363318 5.87 ug/1 # 99 46) Benzo(b)fluoranthene 36.84 252 246810 7.07 ug/1 # 96 47) Benzo(k)fluoranthene 36.92 252 299328 8.53 ug/1 # 97 48) Benzo(a)pyrene 37.85 252 195748 6.76 ug/1 # 95 49) Indeno(l,2,3-cd)pyrene 42.23 276 223010 8.45 ug/1 # 94 50) Dibenz(a,h)anthracene 42.32 278 194459 9.64 ug/1 97 51) Benzo(g,h,i)perylene 43.50 276 199709 9.38 ug/1 94

(#) = qualifier out of range (m) = manual integration REFC.D GCMS0208.M • Mon Mar 25 12:00:49 2002 Page 2

NYC-WTC_000011391

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NYC-WTC_000011391Source: NYC Law Department, mirrored locally

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