GCMS reference analysis results for sample AE03265, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAR0102\REFC2.D Vial: 39 Acq On 3 Mar 2002 1:40 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 6 10:40 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.32 152 243037 20.00 ug/1 -0.04 10) Naphthalene-d8 15.95 136 947636 20.00 ug/1 -0.05 17) Acenaphthene-diO 21.27 164 511937 20.00 ug/1 -0.05 2 9) Phenanthrene-dl0 25.71 188 745085 20.00 ug/1 -0.06 38) Chrysene-dl2 33.78 240 499154 20.00 ug/1 -0.06 44) Perylene-dl2 38.05 264 327914 20.00 ug/1 -0.07

System Monitoring Compounds 37) 2,4-DDD 30.80 235 53205 6.84 ug/mL 0.30 Spiked Amount 5.000 Recovery = 136.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.94 74 57279 5.89 ug/1 # 70 3) bis(2-Chloroethyl)ether 11.70 93 139559 8.74 ug/1 93 4) 1,3-Dichlorobenzene 12.22 146 99758 5.25 ug/1 98 5) 1,4-Dichlorobenzene 12.36 146 107272 5.54 ug/1 99 6) 1,2-Dichlorobenzene 12.88 146 106952 5.81 ug/1 99 7) 2,2'-oxybi s(1-Chioropropan 13.19 45 203631 8.42 ug/1 98 8) N-Nitroso-di-n-propylamine 13.57 70 93360 8.17 ug/1 # 85 9) Hexachloroethane 13.73 117 30513 3.93 ug/1 98 11) Nitrobenzene 14.00 77 127966 6.57 ug/1 95 12) 1sophorone 14.64 82 274643 8.34 ug/1 97 13) bis(2-Chloroethoxy)methane 15.32 93 167936 8.19 ug/1 98 14) 1,2,4-Trichlorobenzene 15.84 180 94239 5.81 ug/1 99 15) Naphthalene 16.02 128 359735 7.13 ug/1 99 16) Hexachlorobutadiene 16.56 225 31585 3.25 ug/1 97 18) Hexachlorocyclopentadiene • 18.75 237 4797 0.65 ug/1 98 19) 2-Chloronaphthalene 19.52 162 215825 7.07 ug/1 98 20) Dimethylphthalate 20.61 163 295568 8.32 ug/1 100 21) 2, 6-Dinitrotoluene 20.83 165 59535 7.39 ug/1 # 85 2 2) Acenaphthylene 20.80 152 326266 7.40 ug/1 100 23) Acenaphthene 21.36 153 237590 7.71 ug/1 98 24) 2,4-Dinitrotoluene 22.00 165 74919 7.34 ug/1 # 78 25) Diethylphthalate 22.75 149 283559 7.68 ug/1 95 26) 4-Chioropheny1-phenylether 22.90 204 122348 7.69 ug/1 95 2 7) Fluorene 22.88 166 262708 7.81 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 23.37 77 270940 6.97 ug/L # 86

(#) = qualifier out of range (m) = manual integration REFC2.D GCMS0208.M Mon Mar 25 12:01:26 2002 Page 1

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