GCMS analysis results for sample AE02595, Mar 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR0 10 2\REF.D Vial: 4 Acq On 1 Mar 2002 11:17 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 4 10:44 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.32 152 266663 20.00 ug/1 -0.04 10) Naphthalene-d8 15.95 136 1034824 20.00 ug/1 -0.05 17) Acenaphthene-diO 21.27 164 560338 20.00 ug/1 -0.05 29) Phenanthrene-dlO 25.71 188 819797 20.00 ug/1 -0.05 38) Chrysene-dl2 33.78 240 572326 20.00 ug/1 -0.06 44) Perylene-dl2 38.05 264 393179 20.00 ug/1 -0.07

System Monitoring Compounds 37) 2,4-DDD 30.80 235 51687 6.04 ug/mL 0.30 Spiked Amount 5.000 Recovery = 120.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.95 74 27845 2.61 ug/1 # 72 3) bis(2-Chloroethyl)ether 11.70 93 65418 3.73 ug/1 94 4) 1,3-Dichlorobenzene 12.22 146 31370 1.50 ug/1 95 5) 1,4-Dichlorobenzene 12.35 146 35331m 1.66 ug'/1 6) 1,2-Dichlorobenzene 12.88 146 37562 1.86 ug/1 98 7) 2,21 -oxybis(1-Chloropropan 13.19 45 96489 3.64 ug/1 97 8) N-Nitroso-di-n-propylamine 13.58 70 44292 3.53 ug/1 # 86 9) Hexachloroethane 13.73 117 5840 0.69 ug/1 95 11) Nitrobenzene 14.00 77 58637 2.76 ug/1 94 12) Isophorone 14.65 82 132146 3.68 ug/1 99 13) bis(2-Chloroethoxy)methane 15.32 93 70985 3.17 ug/1 98 14) 1,2,4-Trichlorobenzene 15.84 180 32813 1.85 ug/1 100 15) Naphthalene 16.02 128 155602 2.82 ug/1 98 16) Hexachlorobutadiene 16.56 225 3532 0.33 ug/1 89 18) Hexachlorocyclopentadiene 18.75 237 553 N.D. 19) 2-Chloronaphthalene 19.52 162 94041 2.81 ug/1 97 20) Dimethylphthalate 20.61 163 140331 3.61 ug/1 99 21) 2,6-Dinitrotoluene 20.83 165 25941 2.94 ug/1 # 85 22) Acenaphthylene 20.80 152 149009 3.09 ug/1 98 23) Acenaphthene 21.36 153 108599 3.22 ug/1 99 24) 2,4-Dinitrotoluene 22.00 165 31523 2.82 ug/1 # 82 25) Diethylphthalate 22.75 149 137645 3.40 ug/1 95 26) 4-Chlorophenyl-phenylether 22.90 204 55868 3.21 ug/1 95 27) Fluorene 22.88 166 121844 3.31 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.37 77 127361 2.99 ug/L # 87

(#) = qualifier out of range (m) = manual integration REF.D GCMS0208.M Mon Mar 04 10:46:49 2002 Page 1

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