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GCMS calibration results, sample AE04948, March 2002

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Laboratory report showing GCMS calibration analysis for volatile organic compounds on March 29, 2002.

NYC-WTC_000058723–000058726

Folder label: “GCMS X 3/7/02 A 3/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR2 602\CAL10.D Vial: 2 Acq On 26 Mar 2002 9:42 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 28 15:05 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.23 168 415086 10.75 ug/1 # 80 31) 4-Bromophenyl-phenylether 24.29 248 257720 11.36 ug/1 91 32) Hexachlorobenzene 24.73 284 304234 11.55 ug/1 # 88 3 3) Phenanthrene 25 ..71 178 1348167 10.93 ug/1 98 34) Anthracene 25.84 178 1272688 10.40 ug/1 99 35) Di-n-butylphthalate 27.61 149 1629641 10.49 ug/1 # 99 36) Fluoranthene 29.33 202 1372012 l£l^&0-^/l 96 3 9) Pyrene 30.00 202 1385010 13^_3>^g/l # 92 40) Butylbenzylphthalate 32.13 149 619017 TTTsS ug/1 98 41) Benzo(a)anthracene 33.65 228 899523 10.44 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 785289 10.88 ug/1 # 94 43) Chrysene 33.78 228 909323 10.76 ug/1 99 45) Di-n-Octylphthalate 35.65 149 1096909 11.87 ug/1 # 98 46) Benzo(b)fluoranthene 36.75 252 713090m 11.14 ug/1 47) Benzo(k)fluoranthene 36.83 252 745353 11.94 ug/1 99 48) Benzo(a)pyrene 37.74 252 574677 9.85 ug/1 # 97 49) Indeno(1,2,3-cd)pyrene 42.07 276 532652 7.56 ug/1 98 50) Dibenz(a,h)anthracene 42.14 278 409917 7.51 ug/l 97 51) Benzo(g,h,i)perylene 43.31 276 449474 7.82 ug/1 98

(#) = qualifier out of range (m) = manual integration CALIO.D GCMS0308.M Fri Mar 29 09:50:12 2002 Page 2

NYC-WTC_000058725

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NYC-WTC_000058725Source: NYC Law Department, mirrored locally

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