GCMS calibration results, sample AE04948, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR26O2\CAL16.D Vial: 2 Acq On 26 Mar 2002 9:42 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 28 15:05 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 I Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.26 152 825079 20.00 ug/1 -0.09 10) Naphthalene-d8 15.89 136 3403289 20.00 ug/1 -0.10 17) Acenaphthene-dlO 21.20 164 1886710 20.00 ug/1 -0.11 29) Phenanthrene-dlO 25.64 188 2857027 20.00 ug/1 -0.12 38) Chrysene-dl2 33.71 240 1804818 20.00 ug/1 -0.13 44) Perylene-dl2 37.95 264 1048495 20.00 ug/1 -0.17

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 275000 9.82 ug/1 # 70 3) bis(2-Chloroethyl)ether 11.67 93 506543 11.24 ug/1 90 4) 1,3.-Dichlorobenzene 12.16 146 501717 10.77 ug/1 98 5) 1,4-Dichlorobenzene 12.30 146 510068 10.93 ug/1 99 6) 1,2-Dichlorobenzene 12.82 146 485516 11.15 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.13 45 663956 10,47 ug/1 99 8) N-Nitroso-di-n-propylamine 13.53 70 322414 10.99 ug/1 # 85 9) Hexachloroethane 13.66 117 186715 10.70 ug/1 93 11) Nitrobenzene 13.95 77 487805 10.48 ug/1 89 12) Isophorone 14.58 82 908390 10.30 ug/1 99 13) bis(2-Chloroethoxy)methane 15.26 93 606018 10.49 ug/1 99 14) 1,2,4-Trichlorobenzene 15.77 180 465332 11.65 ug/1 97 15) Naphthalene 15.95 128 1415919 11.26 ug/1 99 16) Hexachlorobutadiene 16.49 225 236209 11.86 ug/1 99 18) Hexachlorocyclopentadiene 18.68 237 144719 11.33 ug/1 99 19) 2-Chloronaphthalene 19.46 162 884640 10.92 ug/1 95 20) Dimethylphthalate 20.55 163 1026311 10.81 ug/1 . 99 21) 2,6-Dinitrotoluene 20.76 165 239819 10.41 ug/1 # 81 22) Acenaphthylene 20.72 152 1261984 10.90 ug/1 99 23) Acenaphthene 21.29 153 892714 • 11.03 ug/1 99 24) 2,4-Dinitrotoluene 21.93 165 306826 9.95 ug/1 # 79 25) Diethylphthalate 22.69 149 971917 10.55 ug/1 95 26) 4-Chlorophenyl-phenylether 22.83 204 467510 11.84 ug/1 92 27) Fluorene 22.81 166 981719 11.47 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.30 77 940658 9.52 ug/L # 83

(#) = qualifier out of range (m) = manual integration CALIO.D GCMS0308.M Eri Mar 29 09:50:09 2002 Page 1

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