GCMS calibration standard results, sample AE00938, March 1, 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\FEB2102 \CAL4 OB. D Vial: 2 Acq On 23 Feb 2002 10:28 am Operator : Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 27 14:18 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.34 168 668429 35.19 ug/1 # 89 31) 4-Bromophenyl-phenylether 24.40 248 387726 31.58 ug/1 98 32) Hexachlorobenzene 24.84 284 441232 30.69 ug/1 98 3 3) Phenanthrene 25.82 178 2090681 35.68 ug/1 100 34) Anthracene 25.95 178 2013818 35.08 ug/1 100 35) Di-n-butylphthalate 27.71 149 2805561 34.26 ug/1 99 36) Fluoranthene 29.45 202 2132220 36.45 ug/1 # 89 3 9) Pyrene 30.13 202 2152949 37.76 ug/1 # 86 40) Butylbenzylphthalate 32.25 149 1153549 36.54 ug/1 96 41) Benzo(a)anthracene 33.76 228 1577534 37.84 ug/1 100 42) Bis(2-ethylhexyl)phthalate 34.01 149 1441596 33.80 ug/1 96 43) Chrysene 33.90 228 1535410 37.43 ug/1 100 45) Di-n-Octylphthalate 35.77 149 2222392 32.90 ug/1 # 99 46) Benzo(b)fluoranthene 36.90 252 1381226 36.23 ug/1 # 97 47) Benzo(k)fluoranthene 36.98 252 1338055 34.92 ug/1 # 96 48) Benzo(a)pyrene 37.91 252 1201027 38.01 ug/1 # 94 49) Indeno(l,2,3-cd)pyrene 42.35 276 1264736m 43.86 ug/1 50) Dibenz(a,h)anthracene 42.41 278 992389m 45.03 ug/1 51) Benzo(g,h,i)perylene 43.63 276 1040356 44.75 ug/1 # 93

(#) = qualifier out of range (m) = manual integration CAL40B.D GCMS0208.M Wed Feb 27 14:18:50 2002 Page 2

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