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GCMS reference standard results, DEP Labs, Feb 2002

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Reference standard analysis report for GCMS testing verifying instrument performance with specific compound concentrations on February 21, 2002.

NYC-WTC_000009820–000009824

Folder label: “GCMS X 1/22/02 A 2/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB2102\REF.D Vial: 4 Acq On : 21 Feb 2002 5:02 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 ■ MS Integration Params: GOOFY.P Quant Time: Feb 22 8:16 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.31 168 44603 3.00 ug/1 # 85 31) 4-Bromophenyl-phenylether 24.39 248 31216 3.25 ug/1 94 32) Hexachlorobenzene 24.82 284 37922 3.37 ug/1 96 3 3) Phenanthrene 25.80 178 175190 3.82 ug/1 99 34) Anthracene 25.93 178 153457 3.42 ug/1 99 35) Di-n-butylphthalate 27.70 149 240604 3.75 ug/1 99 3 6) Fluoranthene 29.42 202 161454 3.53 ug/1 # 87 3 9) Pyrene 30.10 202 168867 3.74 ug/1 # 86 40) Butylbenzylphthalate 32.23 149 69222 2.77 ug/1 98 41) . Benzo(a)anthracene 33.75 228 114595 3.48 ug/1 100 42) Bis(2-ethylhexyl)phthalate 34.01 149 102877 3.05 ug/1 # 93 43) Chrysene 33.88 228 131556 4.05 ug/1 99 45) Di-n-Octylphthalate 35.75 149 105069 1.86 ug/1 # 97 46) Benzo(b)fluoranthene 36.87 252 93844 2.94 ug/1 # 96 47) Benzo(k)fluoranthene 36.93 252 122754 3.83 ug/1 # 94 48) Benzo(a)pyrene 37.88 252 74565 2.82 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 42.29 276 80086 3.32 ug/1 95 50) Dibenz(a,h)anthracene 42.36 278 67107 3.64 ug/1 # 93 51) Benzo(g,h,i)perylene 43.53 276 75332 3.87 ug/1 # 93

(#) = qualifier out of range (m) = manual integration REF.D GCMS0208.M Fri Feb 22 09:06:10 2002 Page 2

NYC-WTC_000009823

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NYC-WTC_000009823Source: NYC Law Department, mirrored locally

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