GCMS reference standard results, DEP Labs, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) $ Data File : C:\HPCHEM\l\DATA\FEB2102\REF.D Vial: 4 Acq On : 21 Feb 2002 5:02 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 22 8:16 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Feb 21 16:13:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 263164 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 988742 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.29 164 550409 20.00 ug/1 -0.02 29) Phenanthrene-diO 25.73 188 758191 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 514887 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 352918 20.00 ug/1 -0.04

System Monitoring Compounds 37) 2,4-DDD 30.81 235 45450 5.18 ug/mL 0.31 Spiked Amount 5.000 Recovery = 103.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.95 74 27115 2.57 ug/1 # 71 3) bis(2-Chloroethyl)ether 11.72 93 65430 3.78 ug/1 93 4) 1,3-Dichlorobenzene 12.23 146 50474 2.45 ug/1 97 5) 1,4-Dichlorobenzene 12.38 146 53450 2.55 ug/1 99 6) 1,2-Dichlorobenzene 12.90 146 52551 2.64 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.21 45 96198 3.67 ug/1 98 8) N-Nitroso-di-n-propylamine 13.60 70 44775 3.62 ug/1 # 84 9) Hexachloroethane 13.74 117 13777 1.64 ug/1 96 11) Nitrobenzene 14.02 77 57436 2.82 ug/1 98 12) Isophorone 14.66 82 129530 3.77 ug/1 98 13) bis(2-Chloroethoxy)methane 15.34 93 78051 3.65 ug/1 98 14) 1,2,4-Trichlorobenzene 15.85 180 44949 2.66 ug/1 97 15) Naphthalene 16.03 128 169387 3.22 ug/1 99 16) Hexachlorobutadiene 16.58. 225 13236 1.31 ug/1 98 18) Hexachlorocyclopentadiene 18.77 237 2518 0.32 ug/1 88 19) 2-Chloronaphthalene 19.54 162 102599 3.13 ug/1 97 20) Dimethylphthalate 20.63 163 141294 3.70 ug/1 99 21) 2,6-Dinitrotoluene 20.84 165 24677 2.85 ug/1 92 22) Acenaphthylene 20.81 152 155567 3.28 ug/1 99 2 3) Acenaphthene 21.38 153 116268 3.51 ug/1 99 24) 2,4-Dinitrotoluene 22.01 165 30102 2.74 ug/1 # 78 25) Diethylphthalate 22.76 149 140201 3.53 ug/1 96 26) 4-Chlorophenyl-phenylether 22.91 204 58815 3.44 ug/1 98 27) Fluorene 22.90 166 126201 3.49 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.38 77 128743 3.08 ug/L # 88

(#) = qualifier out of range (m) = manual integration REF.D GCMS0208.M Fri Feb 22 09:06:07 2002 Page 1

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