DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB2702\REFA.D Vial: 18 Acq On : 28 Feb 2002 2:21 am Operator: Sample : gc/ms scan 1/31 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 7 15:10 2002 ।Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.32 152 360640 20.00 ug/1 -0.04 10) Naphthalene-d8 15.96 136 1385755 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.28 164 737887 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.72 188 1054798 20.00 ug/1 -0.05 38) Chrysene-dl2 33.79 240 696487 20.00 ug/1 -0.06 44) Perylene-dl2 38.07 264 480278 20.00 ug/1 -0.06

System Monitoring Compounds 37) 2,4-DDD 30.80 235 31770 2.88 ug/mL 0.30 Spiked Amount 5.000 Recovery = 57.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.94 74 18554 1.29 ug/1 # 72 3) bis(2-Chloroethyl)ether 11.71 93 45775 1.93 ug/1 93 4) 1,3-Dichlorobenzene 12.21 146 29882 1.06 ug/1 99 5) 1,4-Dichlorobenzene 12.36 146 32506m 1.13 ug/1 6) 1,2-Dichlorobenzene 12.88 146 32778 1.20 ug/1 99 7) 2,2'-oxybi s(1-Chloropropan 13.20 45 68716 1.91 ug/1 98 8) N-Nitroso-di-n-propylamine 13.58 70 30205 1.78 ug/1 # 86 9) Hexachloroethane 13.73 117 8168 0.71 ug/1 97 11) Nitrobenzene 14.00 77 39514 1.39 ug/1 99 12) 1sophorone 14.65 82 86218 1.79 ug/1 98 13) bis(2-Chloroethoxy)methane 15.33 93 52594 1.75 ug/1 96 14) 1,2,4-Trichlorobenzene 15.84 180 27702 1.17 ug/1 95 15) Naphthalene 16.02 128 118318 1.60 ug/1 98 16) Hexachlorobutadiene 16.56 225 7635 0.54 ug/1 96 18) Hexachlorocyclopentadiene 18.76 237 1202 N.D. 19) 2-Chloronaphthalene 19.53 162 66066 1.50 ug/1 97 20) Dimethylphthalate 20.61 163 94417 1.84 ug/1 99 21) 2,6-Dinitrotoluene 20.83 165 14597 1.26 ug/1 89 22) Acenaphthylene 20.80 152 102474 1.61 ug/1 99 2 3) Acenaphthene 21.36 153 79526 1.79 ug/1 98 24) 2,4-Dinitrotoluene 22.00 165 17185 1.17 ug/1 88 25) Diethylphthalate 22.74 149 92975 1.75 ug/1 97 26) 4-Chlorophenyl-phenylether 22.90 204 39400 1.72 ug/1 98 27) Fluorene 22.88 166 84899 1.75 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.37 77 83518 1.49 ug/L # 89

(#) = qualifier out of range (m) = manual integration REFA.D SW030702.M Wed Mar 20 14:56:53 2002 Page 1

NYC-WTC_000004711