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GCMS analysis results for sample AE03833, Mar 13 2002

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Laboratory report detailing GCMS analysis of sample AE03833 conducted on March 13, 2002.

NYC-WTC_000038257–000038261

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038260
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB2102\REFE2.D Vial: 72 Acq On : 24 Feb 2002 4:53 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 11:09 2002 Quant Results Pile: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenyl amine 23.30 168 85223 6.38 ug/1 # 90 31) 4-Bromophenyl-phenylether 24.39 248 60239 6.98 ug/1 98 3 2) Hexachlorobenzene 24.83 284 71095 7.03 ug/1 95 33) Phenanthrene 25.80 178 344614 8.37 ug/1 100 34) Anthracene 25.93 178 328977 8.15 ug/1 99 35) Di-n-butylphthalate 27.70 149 484056 8.41 ug/1 99 3 6) Fluoranthene 29.43 202 341146 8.30 ug/1 # 88 3 9) Pyrene 30.11 202 352266 8.38 ug/1 # 88 40) Butylbenzylphthalate 32.23 149 176648 7.59 ug/1 92 41) Benzo(a)anthracene 33.75 228 258677 8.42 ug/1 99 42) Bis(2-ethylhexyl)phthalate 34.01 149 228535 7.27 ug/1 96 43) Chrysene 33.88 228 274745 9.09 ug/1 100 45) Di-n-Octylphthalate 35.75 149 280306 5.66 ug/1 98 46) Benzo(b)fluoranthene 36.87 252 225283 8.06 ug/1 # 97 47) Benzo(k)fluoranthene 36.94 252 258518 9.21 ug/1 # 96 48) Benzo(a)pyrene 37.88- 252 177064 7.65 ug/1 # 94 49) Indeno(l,2,3-cd)pyrene 42.28 276 174989 8.28 ug/1 # 92 50) Dibenz(a,h)anthracene 42.35 278 148334 9.18 ug/1 # 92 51) Benzo(g,h,i)perylene 43.55 276 153544 9.01 ug/1 # 93

(#) = qualifier out of range (m) = manual integration REFE2.D GCMS0208.M Wed Mar 13 11:12:12 2002 Page 2

NYC-WTC_000038260

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NYC-WTC_000038260Source: NYC Law Department, mirrored locally

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