GCMS analysis results for sample AE03833, Mar 13 2002

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Data File : C:\HPCHEM\l\DATA\FEB2102\REFE2.D Vial: 72 Acq On : 24 Feb 2002 4:53 pm Operator : Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 11:09 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via :. Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 229525 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 887873 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.28 164 480210 20.00 ug/1 -0.03 29) Phenanthrene-diO 25.74 188 681131 20.00 ug/1 -0.03 38) Chrysene-dl2 33.81 240 479820 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 309165 20.00 ug/1 -0.05

System Monitoring Compounds 37) 2,4-DDD Spiked Amount 5.000 30.81 235 49914 Recovery 44ug/mt = 140.40% 0.32

Target Compounds 82%Qvalue , 2) N-nitroso-dimethyl amine 5.94 74 58356 6.35 ug/1 # 74 3) bis(2-Chloroethyl)ether 11.72 93 138008 9.15 ug/1 95 4) 1,3-Dichlorobenzene 12.23 146 93512 5.21 ug/1 99 5) 1,4-Dichlorobenzene 12.38 146 97558 5.33 ug/1 98 6) 1,2-Dichlorobenzene 12.89 146 98697 5.68 ug'/l 99 7) 2,2’-oxybi s(1-Chioropropan 13.22 45 204064 8.93 ug/1 98 8) N-Nitroso-di-n-propylamine 13.59 70 96694 8.96 ug/1 # 87 9) Hexachloroethane 13.75 117 27983 3.82 ug/1 98 11) Nitrobenzene 14.01 77 126246 6.91 ug/1 96 12) 1sophorone 14.67 82 283456 9.19 ug/1 99 13) bis(2-Chloroethoxy)methane 15.34 93 163623 8.52 ug/1 97 14) 1,2,4-Trichlorobenzene 15.86 180 83615 5.50 ug/1 98 15) Naphthalene 16.03 128 338380 7.16 ug/1 99 16) Hexachiorobutadiene 16.58 225 28610 3.15 ug/1 99 18) Hexachlorocyclopentadiene 18.77 237 10627 1.55 ug/1 96 19) 2-Chloronaphthalene 19.54 162 200833 7.01 ug/1 98 20) Dimethylphthalate 20.62 163 279271 8.38 ug/1 99 21) 2,6-Dinitrotoluene 20.84 165 52735 6.98 ug/1 88 2 2) Acenaphthylene 20.82 152 330744 8.00 ug/1 99 23) Acenaphthene 21.38 153 227652 7.87 ug/1 99 24) 2,4-Dinitrotoluene 22.01 165 63655 6.65 ug/1 # 88 25) Diethylphthalate 22.76 149 285313 8.23 ug/1 97 26) 4-Chlorophenyl-phenylether 22.92 204 113888 7.63 ug/1 98 27) Fluorene 22.90 166 248824 7.89 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 23.39 77 268926 7.38 ug/L # 89

(#) = qualifier out of range (m) = manual integration REFE2.D GCMS0208.M Wed Mar 13 11:12:08 2002 Page 1

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