DEP GCMS method 608 data sheet, Feb 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\FEB2 5 0 2\CAL2 5A.D Vial: 2 Acq On 26 Feb 2002 1:33 pm Operator : Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 28 11:12 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 310604 20.00 ug/1 -0.03 10) Naphthalene-d8 15.97 136 1203212 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.28 164 641208 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.73 188 964253 20.00 ug/1 -0.04 38) Chrysene-dl 2 33.80 240 681292 20.00 ug/1 -0.05 44) Perylene-dl2 38.07 264 478831 20.00 ug/1 -0.06

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.94 74 367418 29.56 ug/1 # 73 3) bis(2-Chloroethyl)ether 11.73 93 556828 27.28 ug/1 94 4) 1,3-Dichlorobenzene 12.22 146 581424 23.93 ug/1 99 5) 1,4-Dichlorobenzene 12.37 146 589913 23.82 ug/1 100 6) 1,2-Dichlorobenzene 12.89 146 547614 23.27 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.21 45 795153 25.73 ug/1 99 8) N-Nitroso-di-n-propylamine 13.60 70 381427 26.12 ug/1 # 88 9) Hexachloroethane 13.73 117 221332 22.33 ug/1 96 11) Nitrobenzene 14.01 77 560464 22.65 ug/1 95 12) Isophorone 14.66 82 1056568 25.28 ug/1 98 13) bis(2-Chloroethoxy)methane 15.34 93 673552 25.88 ug/1 97 14) 1,2,4-Trichlorobenzene 15.85 180 476116 23.12 ug/1 98 15) Naphthalene 16.02 128 1516342 23.66 ug/1 99 16) Hexachlorobutadiene 16.57 225 247953 20.12 ug/1 99 18) Hexachlorocyclopentadiene 18.76 237 193793 21.11 ug/1 98 19) 2-Chloronaphthalene 19.53 162 917049 23.99 ug/1 98 20) Dimethylphthalate 20.62 163 1070557 24.05 ug/1 100 21) 2,6-Dinitrotoluene 20.84 165 252954 25.07 ug/1 # 83 22) Acenaphthylene 20.81 152 1335625 24.18 ug/1 99 23) Acenaphthene 21.38 153 927513 24.03 ug/1 98 24) 2,4-Dinitrotoluene 22.01 165 331334 25.92 ug/1 # 82 25) Diethylphthalate 22.76 149 1051762 22.73 ug/1 97 26) 4-Chlorophenyl-phenylether 22.91 204 461124 23.15 ug/1 95 27) Fluorene 22.89 166 991691 23.54 ug/1 98 28) Azobenzen/ 1,2-Diphenylhyd 23.38 77 1076828 22.12 ug/L # 90

(#) = qualifier out of range (m) = manual integration CAL25A.D GCMS0208.M Thu Feb 28 11:16:00 2002 Page 1

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