GCMS calibration results for volatile organics, February 2002

NYC 9/11 Public Portal Document

• Data File C:\HPCHEM\1\DATA\FEB1102\CAL8 0.D Vial: 2 Acq On 11 Feb 2002 11:12 am Operator: 209 GALOS b Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 19 9:41 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.36 152 348393 20.00 ug/1 0.00 10) Naphthalene-d8 16.01 136 1325869 20.00 ug/1 0.01 17) Acenaphthene-dlO 21.32 164 759459 20.00 ug/1 0.00 29) Phenanthrene-dlO 25.78 188 1036754 20.00 ug/1 0.01 38) Chrysene-dl2 33.86 240 801918 20.00 ug/1 0.01 44) Perylene-dl2 38.14 264 498183 20.00 ug/1 0.01

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds 2) N-nitroso-dimethyl amine 6.00 74 1149161 04P 82.43 ug/1 Qvalue 92 3) bis(2-Chloroethyl)ether 11.78 93 1964680 85.80 ug/1 97 4) 1,3-Dichlorobenzene 12.27 146 2268701 83.24 ug/1 100 5) 1,4-Dichlorobenzene 12.40 146 2338545 84.18 ug/1 98 6) 1,2-Dichlorobenzene 12.93 146 2211671 83.79 ug/1 100 7) 2,21-oxybis(1-Chloropropan 13.25 45 2976228 85.85 ug/1 99 8) N-Nitroso-di-n-propylamine 13.68 70 1392883 85.02 ug/1 94 9) Hexachloroethane 13.77 117 921243 82.85 ug/1 99 11) Nitrobenzene 14.07 77 2214381 81.22 ug/1 99 12) Isophorone 14.74 82 3890980 84.48 ug/1 99 13) bis(2-Chloroethoxy)methane 15.40 93 2477348 86.37 ug/1 100 14) 1,2,4-Trichlorobenzene 15.89 180 1875356 82.65 ug/1 98 15) Naphthalene 16.08 128 6019292 85.24 ug/1 100 16) Hexachlorobutadiene 16.60 225 1094813 80.63 ug/1 100 18) Hexachlorocyclopentadiene 18.80 237 929518 85.49 ug/1 100 19) 2-Chloronaphthalene 19.59 162 3693799 81.58 ug/1 98 20) Dimethylphthalate 20.69 163 4268893 80.95 ug/1 100 21) 2,6-Dinitrotoluene 20.91 165 1002456 83.87 ug/1 91 22) Acenaphthylene 20.86 152 5444753 83.24 ug/1 100 23) Acenaphthene 21.44 153 3765193 82.35 ug/1 99 24) 2,4-Dinitrotoluene 22.09 165 1273664 84.12 ug/1 93 25) Diethylphthalate 22.83 149 4451283 81.22 ug/1 99 26) 4-Chlorophenyl-phenylether 22.97 204 1861116 78.89 ug/1 96 27) Fluorene 22.96 166 4031104 80.79 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.45 77 5145786 89.26 ug/L 91

(#) = qualifier out of range (m) = manual integration CALS 0.D GCMS0208.M Tue Feb 19 09:41:34 2002 Page 1

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