GCMS reference results for sample AE01041, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1502\REFB.D Vial: 25 Acq On : 16 Feb 2002 4:40 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 20 12:35 2002 <Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Diehlorobenzene-d4 12.33 152 260745 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 991731 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.29 164 531869 20.00 ug/1 -0.02 29) Phenanthrene-dlO 25.73 188 748465 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 509444 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 353687 20.00 ug/1 -0.04

System Monitoring Compounds 37) 2,4-DDD 30.82 235 29872 3.98 ug/mL 0.32 Spiked Amount 5.000 Recovery = 79.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.96 74 14027 1.34 ug/1 98 3) bis(2-Chloroethyl)ether 11.72 93 36550 2.13 ug/1 96 4) 1,3-Dichlorobenzene 12.23 146 32012 1.57 ug/1 95 5) 1,4-Dichlorobenzene 12.38 146 33759 1.62 ug/1 98 6) 1,2-Dichlorobenzene 12.89 146 33166 1.68 ug/1 100 7) 2,21-oxybis(1-Chloropropan 13.21 45 60244 2.32 ug/1 97 8) N-Nitroso-di-n-propylamine 13.60 70 28266 2.31 ug/1 95 9) Hexachloroethane 13.74 117 10145 1.22 ug/1 91 11) Nitrobenzene 14.02 77 35230 1.73 ug/1 98 12) 1sophorone 14.66 82 78056 2.27 ug/1 98 13) bis(2-Chloroethoxy)methane 15.34 93 46774 2.18 ug/1 98 14) 1,2,4-Trichlorobenzene 15.85 180 30145 1.78 ug/1 98 15) Naphthalene 16.03 128 110123 2.09 ug/1 100 16) Hexachlorobutadiene 16.57 225 11441 1.13 ug/1 96 18) Hexachlorocyclopentadiene 18.77 237 2312 0.30 ug/1 # 84 19) 2-Chloronaphthalene 19.55 162 69467 2.19 ug/1 97 20) Dimethylphthalate 20.63 163 96962 2.63 ug/1 99 21) 2,6-Dinitrotoluene 20.84 165 13141 1.57 ug/1 # 85 22) Acenaphthylene 20.81 152 99444 2.17 ug/1 99 2 3) Acenaphthene 21.38 153 78275 2.44 ug/1 98 24) 2,4-Dinitrotoluene 22.01 165 16337 1.54 ug/1 95 25) Diethylphthalate 22.76 149 101960 2.66 ug/1 98 26) 4-Chlorophenyl-phenylether 22.92 204 41833 2.53 ug/1 98 27) Fluorene 22.90 166 85219 2.44 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.38 77 91806 2.27 ug/L 97

(#) = qualifier out of range (m) = manual integration REFB.D GCMS0208.M Wed Feb 20 14:02:45 2002 Page 1

NYC-WTC_000052787