GCMS calibration results for sample AE01330, Feb 2002

NYC 9/11 Public Portal Document

L\SpOL L (V1 Kevlewed)

Data File C:\HPCHEM\1\DATA\FEB19 0 2\CAL10.D Vial: 2 Acq On 19 Feb 2002 10:15 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 21 12:33 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 258253 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 987073 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.29 164 519570 20.00 ug/1 -0.02 29) Phenanthrene-diO 25.73 188 737676 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 510354 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 338386 20.00 ug/1 -0.04

System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.95 74 123405 11.94 ug/1 # 69 3) bis(2-Chloroethyl)ether 11.73 93 199156 11.73 ug/1 93 4) 1,3-Dichlorobenzene 12.23 146 205787 10.19 ug/1 98 5) 1,4-Dichlorobenzene 12.38 146 209019 10.15 ug/1 98 6) 1,2-Dichlorobenzene 12.90 146 191314 9.78 ug/1 97 7) 2,2'-oxybis(1-Chloropropan 13.21 45 292690 11.39 ug/1 98 8) N-Nitroso-di-n-propylamine 13.60 70 127662 10.51 ug/1 # 85 9) Hexachloroethane 13.74 117 73822 8.96 ug/1 98 11) Nitrobenzene 14.02 77 190109 9.37 ug/1 93 12) Isophorone 14.66 82 358500 10.46 ug/1 97 13) bis (2-Chloroethoxy)methane 15.34 93 236731 11.09 ug/1 97 14) 1,2,4-Trichlorobenzene 15.86 180 157432 9.32 ug/1 98 15) Naphthalene 16.03 128 529865 10.08 ug/1 99 16) Hexachlorobutadiene 16.57 225 82226 813 ug/1 99 18) Hexachlorocyclopentadiene 18.77 237 58597 (7.88 ug/1 98 19) 2-Chloronaphthalene 19.55 162 312910 10.10 ug/1 97 20) Dimethylphthalate 20.63 163 360351 9.99 ug/1 100 21) 2,6-Dinitrotoluene 20.84 165 82172 10.05 ug/1 # 84 22) Acenaphthylene 20.81 152 465427 10.40 ug/1 99 23) Acenaphthene 21.38 153 319219 10.21 ug/1 98 24) 2,4-Dinitrotoluene 22.02 165 105878 10.22 ug/1 # 76 25) Diethylphthalate 22.77 149 361059 9.63 ug/1 97 26) 4-Chlorophenyl-phenylether 22.92 204 151625 9.39 ug/1 96 27) Fluorene 22.90 166 334127 9.79 ug/1 97 28) Azobenzen/ 1,2-Diphenylhyd 23.39 77 373535 9.47 ug/L # 85

(#) = qualifier out of range (m) = manual integration AL10.D GCMS0208.M Thu Feb 21 12:35:29 2002 Page 1

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